N-methyl-N-phenylcarbamoylsulfenyl-1-β-mercapto-β,β-cyclopentamethylenepropionic acid

Base Information

• Chemical Name: N-methyl-N-phenylcarbamoylsulfenyl-1-β-mercapto-β,β-cyclopentamethylenepropionic acid
• CAS No.: 256229-75-1
• Molecular Formula: C₁₆H₂₁NO₃S₂
• Molecular Weight: 339.48

Synonyms:N-methyl-N-phenylcarbamoylsulfenyl-1-β-mercapto-β,β-cyclopentamethylenepropionic acid

Chemical Property of N-methyl-N-phenylcarbamoylsulfenyl-1-β-mercapto-β,β-cyclopentamethylenepropionic acid

Chemical Property:

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Technology Process of N-methyl-N-phenylcarbamoylsulfenyl-1-β-mercapto-β,β-cyclopentamethylenepropionic acid

There total 3 articles about N-methyl-N-phenylcarbamoylsulfenyl-1-β-mercapto-β,β-cyclopentamethylenepropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methylaniline (100-61-8) + C9H13ClO3S2 → N-methyl-N-phenylcarbamoylsulfenyl-1-β-mercapto-β,β-cyclopentamethylenepropionic acid (256229-75-1)

Guidance literature:

In chloroform; at 0 ℃; for 0.5h;

DOI:10.1021/jm9900220

Reference yield:

[1-(acetylamino-methylsulfanyl)-cyclohexyl]-acetic acid → N-methyl-N-phenylcarbamoylsulfenyl-1-β-mercapto-β,β-cyclopentamethylenepropionic acid (256229-75-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CHCl₃ / 0.25 h / 0 - 5 °C

2: CHCl₃ / 0.5 h / 0 °C

In chloroform; 1: Substitution / 2: Acylation;

DOI:10.1021/jm9900220

Reference yield:

S-4-methylbenzyl-1-β-mercapto-β,β-cyclopentamethylenepropionic acid → N-methyl-N-phenylcarbamoylsulfenyl-1-β-mercapto-β,β-cyclopentamethylenepropionic acid (256229-75-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CHCl₃ / 0.25 h / 0 - 5 °C

2: CHCl₃ / 0.5 h / 0 °C

In chloroform; 1: Substitution / 2: Acylation;

DOI:10.1021/jm9900220

upstream raw materials:

N-methylaniline

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