2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan

Base Information

Chemical Name:2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan
CAS No.:80431-36-3
Molecular Formula:C₂₅H₄₃NSi₄
Molecular Weight:469.965
Hs Code.:

Synonyms:2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan

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Chemical Property of 2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan

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Technology Process of 2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan

There total 6 articles about 2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 80431-44-3
2,3,4,4a-Tetrahydro-3,3-dimethyl-1-phenyl-2,4,4-tris(trimethylsilyl)-2-aza-3-silanaphthalin

: 80431-36-3
2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan

Guidance literature:: In diethyl ether; at 110 ℃; for 5h;

Reference yield:

: 62139-74-6
Brom(bromdimethylsilyl)bis(trimethylsilyl)methan

: 80431-36-3
2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / ZnF₂ / diethyl ether / 8 h / 170 °C

2: 1.) n-BuLi/hexane / 1.) Et₂O/hexane, -78 deg C to -10 deg C, 2.) Et₂O, -78 deg C to room temp.

With n-butyllithium; zinc(II) fluoride; hexane; In diethyl ether;

Reference yield:

: 78907-38-7
Brom(fluordimethylsilyl)bis(trimethylsilyl)methan

: 80431-36-3
2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi/hexane / 1.) Et₂O/hexane, -78 deg C to -10 deg C, 2.) Et₂O, -78 deg C to room temp.

2: diethyl ether / 80 °C / further temperatures, further solvents, ΔG, ΔH, ΔS, τ_1/2, ΔG(excit), ΔH(excit), ΔS(excit); prod. yield distribution

With n-butyllithium; hexane; In diethyl ether;