3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Base Information

Chemical Name:3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate
CAS No.:1096154-19-6
Molecular Formula:C₂₆H₂₄Cl₃NO₉
Molecular Weight:600.837
Hs Code.:

Synonyms:3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

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Chemical Property of 3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

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Technology Process of 3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

There total 4 articles about 3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1096154-35-6
3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranose

: 545-06-2
trichloroacetonitrile

: 1096154-19-6
3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1016/j.carres.2008.09.010

Reference yield:

: 583041-01-4
4-methoxyphenyl 4-O-benzoyl-α-L-rhamnopyranoside

: 1096154-19-6
3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane / Inert atmosphere

2: pyridine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

3: ammonium cerium (IV) nitrate / acetonitrile / 0.33 h / 35 °C

4: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0 °C / Inert atmosphere

With pyridine; ammonium cerium (IV) nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; acetonitrile;
DOI:10.1080/07328301003786789

Reference yield:

: 1096154-18-5
4-methoxyphenyl 3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranoside

: 1096154-19-6
3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium cerium (IV) nitrate / acetonitrile / 0.33 h / 35 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0 °C / Inert atmosphere

With ammonium cerium (IV) nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; acetonitrile;
DOI:10.1080/07328301003786789