(4R)-3-({3-[(tert-butoxy)carbonyl]amino}-1-oxopropyl)-4-isopropyl-5,5-diphenyloxazolidin-2-one

Base Information

Chemical Name:(4R)-3-({3-[(tert-butoxy)carbonyl]amino}-1-oxopropyl)-4-isopropyl-5,5-diphenyloxazolidin-2-one
CAS No.:637337-49-6
Molecular Formula:C₂₆H₃₂N₂O₅
Molecular Weight:452.55
Hs Code.:

Synonyms:(4R)-3-({3-[(tert-butoxy)carbonyl]amino}-1-oxopropyl)-4-isopropyl-5,5-diphenyloxazolidin-2-one

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Chemical Property of (4R)-3-({3-[(tert-butoxy)carbonyl]amino}-1-oxopropyl)-4-isopropyl-5,5-diphenyloxazolidin-2-one

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Technology Process of (4R)-3-({3-[(tert-butoxy)carbonyl]amino}-1-oxopropyl)-4-isopropyl-5,5-diphenyloxazolidin-2-one

There total 1 articles about (4R)-3-({3-[(tert-butoxy)carbonyl]amino}-1-oxopropyl)-4-isopropyl-5,5-diphenyloxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 3303-84-2
3-(tert-butyloxycarbonylamino)propionic acid

: 191090-32-1
(R)-4-(1-methylethyl)-5,5-diphenyl-1,3-oxazolidin-2-one

: 637337-49-6
(4R)-3-({3-[(tert-butoxy)carbonyl]amino}-1-oxopropyl)-4-isopropyl-5,5-diphenyloxazolidin-2-one

Guidance literature:: 3-(tert-butyloxycarbonylamino)propionic acid; With pivaloyl chloride; triethylamine; In tetrahydrofuran; at -30 ℃; for 2h;

(R)-4-(1-methylethyl)-5,5-diphenyl-1,3-oxazolidin-2-one; With lithium chloride; In tetrahydrofuran; at -30 ℃; for 36h;
DOI:10.1002/hlca.200590157

Reference yield: 91.0%

: 75-07-0,9002-91-9
acetaldehyde

: 637337-49-6
(4R)-3-({3-[(tert-butoxy)carbonyl]amino}-1-oxopropyl)-4-isopropyl-5,5-diphenyloxazolidin-2-one

: 637337-09-8
(4R)-[(2R,3S)-2-({[(tert-butoxy)carbonyl]amino}methyl)-3-hydroxy-1-oxopropyl]-4-(1-methylethyl)-5,5-diphenyloxazolidin-2-one

Guidance literature:: With di-n-butylboryl trifluoromethanesulfonate; triethylamine;
DOI:10.1002/hlca.200390149

Reference yield:

: 75-07-0,9002-91-9
acetaldehyde

: 637337-49-6
(4R)-3-({3-[(tert-butoxy)carbonyl]amino}-1-oxopropyl)-4-isopropyl-5,5-diphenyloxazolidin-2-one

: (4R)-[(2S,3S)-2-({[(tert-butoxy)carbonyl]amino}methyl)-3-hydroxy-1-oxopropyl]-4-(1-methylethyl)-5,5-diphenyloxazolidin-2-one

: 637337-09-8
(4R)-[(2R,3S)-2-({[(tert-butoxy)carbonyl]amino}methyl)-3-hydroxy-1-oxopropyl]-4-(1-methylethyl)-5,5-diphenyloxazolidin-2-one

Guidance literature:: (4R)-3-({3-[(tert-butoxy)carbonyl]amino}-1-oxopropyl)-4-isopropyl-5,5-diphenyloxazolidin-2-one; With di-n-butylboryl trifluoromethanesulfonate; triethylamine; In dichloromethane; at -78 ℃; for 1h;

acetaldehyde; In dichloromethane; at -78 - 0 ℃;
DOI:10.1002/hlca.200590157