1-Phenyl-1-nonyne

Base Information

Chemical Name:1-Phenyl-1-nonyne
CAS No.:57718-18-0
Molecular Formula:C15H20
Molecular Weight:200.324
Hs Code.:2902909090
DSSTox Substance ID:DTXSID00206424
Nikkaji Number:J208.850I
Wikidata:Q83080255
Mol file:57718-18-0.mol

Synonyms:1-Phenyl-1-nonyne;57718-18-0;non-1-ynylbenzene;non-1-yn-1-ylbenzene;1-Nonynylbenzene;1-Nonynylbenzene #;Non-1-ynyl-benzene;1-Heptyl-2-phenylacetylene;DTXSID00206424;ZRQWNFWWPPYNFA-UHFFFAOYSA-N;MFCD00048944;AKOS015840581;BS-22719;P0363;T72649

Suppliers and Price of 1-Phenyl-1-nonyne

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-Phenyl-1-nonyne
50mg
$ 45.00

TCI Chemical
1-Phenyl-1-nonyne >98.0%(GC)
5mL
$ 256.00

Rieke Metals
Non-1-ynyl-benzene
5g
$ 1728.00

GFS CHEMICALS
1-PHENYL-1-NONYNE
5 G
$ 536.70

AK Scientific
1-Phenyl-1-nonyne
5ml
$ 460.00

Total 13 raw suppliers

Chemical Property of 1-Phenyl-1-nonyne

Chemical Property:

Refractive Index:1.5180 to 1.5220
Boiling Point:295.2°Cat760mmHg
Flash Point:128.3°C
PSA：0.00000
Density:0.9g/cm³
LogP:4.39860
XLogP3:5.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:6
Exact Mass:200.156500638
Heavy Atom Count:15
Complexity:197

Purity/Quality:

98% ^*data from raw suppliers

1-Phenyl-1-nonyne ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCC#CC1=CC=CC=C1

Technology Process of 1-Phenyl-1-nonyne

There total 6 articles about 1-Phenyl-1-nonyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 591-51-5
phenyllithium

: 189343-67-7
1-(benzotriazol-1-yl)-1-phenoxy-2-nonanone p-tosylhydrazone

: 57718-18-0
non-1-yn-1-ylbenzene

Guidance literature:: In diethyl ether; 1) -78 deg C, 0.5 h; 2) rt, 48 h;
DOI:10.1021/jo962291t

Reference yield: 74.0%

: 6738-06-3
phenylethynylmagnesium bromide

: 4282-40-0
1-Iodoheptane

: 57718-18-0
non-1-yn-1-ylbenzene

Guidance literature:: With Bis<2-(N,N-dimethylamino)aethyl>aether; iron(II) bromide; In tetrahydrofuran; at 20 ℃; for 16h; Solvent; Inert atmosphere; Glovebox;
DOI:10.1021/ol501087m

Reference yield:

: 106-32-1
octanoic acid ethyl ester

: 57718-18-0
non-1-yn-1-ylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / n-BuLi / tetrahydrofuran; hexane / 12 h / -78 - 20 °C

2: 95 percent / Amberlyst-15 / benzene / 12 h / Heating

3: 83 percent / diethyl ether / 1) -78 deg C, 0.5 h; 2) rt, 48 h

With n-butyllithium; amberlyst-15; In tetrahydrofuran; diethyl ether; hexane; benzene;
DOI:10.1021/jo962291t