C₂₆H₂₉NO₅Se

Base Information

• Chemical Name: C₂₆H₂₉NO₅Se
• CAS No.: 470465-31-7
• Molecular Formula: C₂₆H₂₉NO₅Se
• Molecular Weight: 514.48
• Mol file: 470465-31-7.mol

Synonyms:C₂₆H₂₉NO₅Se

Chemical Property of C₂₆H₂₉NO₅Se

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₉NO₅Se

There total 21 articles about C₂₆H₂₉NO₅Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

diphenyl diselenide (1666-13-3) + C20H23NO5 (470465-30-6) → C26H29NO5Se (470465-31-7)

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 2h; Heating;

DOI:10.1021/ja027882h

Reference yield:

C24H27NO5S → C26H29NO5Se (470465-31-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 70 percent / boron tribromide / CH₂Cl₂ / 1 h / -40 °C

2: Red-Al / toluene / 0.5 h / Heating

3: 77 mg / Et₃N / CH₂Cl₂ / 1 h / 25 °C

4: 75 percent / hydrogen peroxide / [(C₈H₁₇)3NCH₃]⁺3[PO₄[W(O)(O₂)2]4]^3- / 1,2-dichloro-ethane; H₂O / 2 h / Heating

5: 75 percent / sodium borohydride / ethanol / 2 h / Heating

With sodium tetrahydroborate; dihydrogen peroxide; boron tribromide; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; [(C₈H₁₇)3NCH₃]⁺3[PO₄[W(O)(O₂)2]4]^3-; In ethanol; dichloromethane; water; 1,2-dichloro-ethane; toluene;

DOI:10.1021/ja027882h

Reference yield:

C24H25NO5S → C26H29NO5Se (470465-31-7)

Guidance literature:

Multi-step reaction with 6 steps

1: 92 percent / sodium borohydride / ethanol / 1 h / 0 °C

2: 70 percent / boron tribromide / CH₂Cl₂ / 1 h / -40 °C

3: Red-Al / toluene / 0.5 h / Heating

4: 77 mg / Et₃N / CH₂Cl₂ / 1 h / 25 °C

5: 75 percent / hydrogen peroxide / [(C₈H₁₇)3NCH₃]⁺3[PO₄[W(O)(O₂)2]4]^3- / 1,2-dichloro-ethane; H₂O / 2 h / Heating

6: 75 percent / sodium borohydride / ethanol / 2 h / Heating

With sodium tetrahydroborate; dihydrogen peroxide; boron tribromide; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; [(C₈H₁₇)3NCH₃]⁺3[PO₄[W(O)(O₂)2]4]^3-; In ethanol; dichloromethane; water; 1,2-dichloro-ethane; toluene;

DOI:10.1021/ja027882h

upstream raw materials:

diphenyl diselenide

C₂₀H₂₃NO₅

5,6-dimethoxy-2-tetralone

1,6-dibromo-2-naphthol

Downstream raw materials:

MORPHIN