2-[(4-nitro-benzenesulfonylamino)-(S)-phenyl-methyl]-acrylic acid methyl ester

Base Information

• Chemical Name: 2-[(4-nitro-benzenesulfonylamino)-(S)-phenyl-methyl]-acrylic acid methyl ester
• CAS No.: 851759-50-7
• Molecular Formula: C₁₇H₁₆N₂O₆S
• Molecular Weight: 376.39

Synonyms:2-[(4-nitro-benzenesulfonylamino)-(S)-phenyl-methyl]-acrylic acid methyl ester

Chemical Property of 2-[(4-nitro-benzenesulfonylamino)-(S)-phenyl-methyl]-acrylic acid methyl ester

Chemical Property:

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Technology Process of 2-[(4-nitro-benzenesulfonylamino)-(S)-phenyl-methyl]-acrylic acid methyl ester

There total 2 articles about 2-[(4-nitro-benzenesulfonylamino)-(S)-phenyl-methyl]-acrylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitro-N-(phenylmethylene)benzenesulfonamide (63160-16-7) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → 2-[(4-nitro-benzenesulfonylamino)-(S)-phenyl-methyl]-acrylic acid methyl ester (851759-50-7) + 2-[(4-nitro-benzenesulfonylamino)-(R)-phenyl-methyl]-acrylic acid methyl ester

Guidance literature:

With TQO; In dichloromethane; at 0 ℃; for 72h; Title compound not separated from byproducts;

DOI:10.1002/chem.200400872

Reference yield:

1,4-diaza-bicyclo[2.2.2]octane (280-57-9,88935-43-7) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) + 4-nitro-N-[(1E)-phenylmethylidene]benzene-1-sulfonamide (63160-16-7) → 2-[(4-nitro-benzenesulfonylamino)-(S)-phenyl-methyl]-acrylic acid methyl ester (851759-50-7) + 2-[(4-nitro-benzenesulfonylamino)-(R)-phenyl-methyl]-acrylic acid methyl ester + C23H28N4O6S + C23H28N4O6S

Guidance literature:

L-tLeu-(Bn)(Me)amide-NH-CS-NH-(R,R)-C₆H₁₀-2-N=CH-derivative; In xylene; at 4 ℃; for 36h; Further Variations:; Catalysts; Solvents; Reagents; equivalents of catalyst, solvent, reaction partner; Product distribution;

DOI:10.1002/adsc.200505230

Reference yield: 92.0%

2-[(4-nitro-benzenesulfonylamino)-(S)-phenyl-methyl]-acrylic acid methyl ester (851759-50-7) → 2-[(4-nitro-benzenesulfonylamino)-(S)-phenyl-methyl]-acrylic acid

Guidance literature:

With hydrogenchloride; for 2h; Heating;

DOI:10.1002/adsc.200505230

upstream raw materials:

4-nitro-N-(phenylmethylene)benzenesulfonamide

acrylic acid methyl ester

1,4-diaza-bicyclo[2.2.2]octane

4-nitro-N-[(1E)-phenylmethylidene]benzene-1-sulfonamide

Downstream raw materials:

(2R,3R)-2-methyl-3-(4-nitrobenzenesulfonylamino)-3-phenyl-propionic acid methyl ester

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