C₃₁H₃₅NO₇

Base Information

• Chemical Name: C₃₁H₃₅NO₇
• CAS No.: 1588418-43-2
• Molecular Formula: C₃₁H₃₅NO₇
• Molecular Weight: 533.621
• Mol file: 1588418-43-2.mol

Synonyms:C₃₁H₃₅NO₇

Chemical Property of C₃₁H₃₅NO₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₃₅NO₇

There total 7 articles about C₃₁H₃₅NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C31H33NO6 (1588418-41-0) → C31H35NO7 (1588418-43-2)

Guidance literature:

C₃₁H₃₃NO₆; With borane-THF; In tetrahydrofuran; at 20 ℃;

With dihydrogen peroxide; sodium hydroxide;

DOI:10.1021/jo500013e

Reference yield:

2-(2,3,6,7-tetramethoxyphenanthren-9-yl)acetonitrile (1554555-42-8) → C31H35NO7 (1588418-43-2)

Guidance literature:

Multi-step reaction with 6 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 2.5 h / 20 °C

2.1: copper(II) sulfate / dichloromethane / 48 h / 20 °C

3.1: zinc; indium(III) triflate / tetrahydrofuran / 20 °C / Inert atmosphere

4.1: hydrogenchloride / methanol; water / 10 h / 0 °C

5.1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C

5.2: 2 h / 0 °C

6.1: borane-THF / tetrahydrofuran / 20 °C

With indium(III) triflate; hydrogenchloride; borane-THF; diisobutylaluminium hydride; potassium carbonate; copper(II) sulfate; zinc; In tetrahydrofuran; methanol; hexane; dichloromethane; water;

DOI:10.1021/jo500013e

Reference yield:

C23H27NO4 (1588418-39-6) → C31H35NO7 (1588418-43-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C

1.2: 2 h / 0 °C

2.1: borane-THF / tetrahydrofuran / 20 °C

With borane-THF; potassium carbonate; In tetrahydrofuran; water;

DOI:10.1021/jo500013e

upstream raw materials:

C₂₃H₂₇NO₄

C₃₁H₃₃NO₆

2-(2,3,6,7-tetramethoxyphenanthren-9-yl)acetonitrile

9-(bromomethyl)-2,3,6,7-tetramethoxyphenanthrene

Downstream raw materials:

(R)-tylophorine

C₃₂H₃₇NO₉S