5-{4-[4-(1-butyl-but-3-enyl)-3,5-dimethoxy-phenyl]-3-methyl-butane-1-sulfonyl}-1-phenyl-1H-tetrazole

Base Information

• Chemical Name: 5-{4-[4-(1-butyl-but-3-enyl)-3,5-dimethoxy-phenyl]-3-methyl-butane-1-sulfonyl}-1-phenyl-1H-tetrazole
• CAS No.: 331273-74-6
• Molecular Formula: C₂₈H₃₈N₄O₄S
• Molecular Weight: 526.7

Synonyms:5-{4-[4-(1-butyl-but-3-enyl)-3,5-dimethoxy-phenyl]-3-methyl-butane-1-sulfonyl}-1-phenyl-1H-tetrazole

Chemical Property of 5-{4-[4-(1-butyl-but-3-enyl)-3,5-dimethoxy-phenyl]-3-methyl-butane-1-sulfonyl}-1-phenyl-1H-tetrazole

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Technology Process of 5-{4-[4-(1-butyl-but-3-enyl)-3,5-dimethoxy-phenyl]-3-methyl-butane-1-sulfonyl}-1-phenyl-1H-tetrazole

There total 4 articles about 5-{4-[4-(1-butyl-but-3-enyl)-3,5-dimethoxy-phenyl]-3-methyl-butane-1-sulfonyl}-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

5-{4-[4-(1-butyl-but-3-enyl)-3,5-dimethoxy-phenyl]-3-methyl-butylsulfanyl}-1-phenyl-1H-tetrazole (331273-75-7) → 5-{4-[4-(1-butyl-but-3-enyl)-3,5-dimethoxy-phenyl]-3-methyl-butane-1-sulfonyl}-1-phenyl-1H-tetrazole (331273-74-6)

Guidance literature:

With ammonium molybdate tetrahydrate; dihydrogen peroxide; In ethanol; at 0 - 20 ℃;

DOI:10.1021/ja003745d

Reference yield:

1-Phenyl-1H-tetrazole-5-thiol (86-93-1) → 5-{4-[4-(1-butyl-but-3-enyl)-3,5-dimethoxy-phenyl]-3-methyl-butane-1-sulfonyl}-1-phenyl-1H-tetrazole (331273-74-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / PPh₃; diethyl azodicarboxylate / tetrahydrofuran / 0.33 h / 20 °C

2: 87 percent / ammonium heptamolybdate tetrahydrate; aq. H₂O₂ / ethanol / 0 - 20 °C

With ammonium molybdate tetrahydrate; dihydrogen peroxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; 1: Mitsunobu reaction;

DOI:10.1021/ja003745d

Reference yield:

(R)-4-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-3-methyl-butan-1-ol (331273-71-3) → 5-{4-[4-(1-butyl-but-3-enyl)-3,5-dimethoxy-phenyl]-3-methyl-butane-1-sulfonyl}-1-phenyl-1H-tetrazole (331273-74-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / PPh₃; diethyl azodicarboxylate / tetrahydrofuran / 0.33 h / 20 °C

2: 87 percent / ammonium heptamolybdate tetrahydrate; aq. H₂O₂ / ethanol / 0 - 20 °C

With ammonium molybdate tetrahydrate; dihydrogen peroxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; 1: Mitsunobu reaction;

DOI:10.1021/ja003745d

upstream raw materials:

5-{4-[4-(1-butyl-but-3-enyl)-3,5-dimethoxy-phenyl]-3-methyl-butylsulfanyl}-1-phenyl-1H-tetrazole

1-Phenyl-1H-tetrazole-5-thiol

(R)-4-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-3-methyl-butan-1-ol

2-((S)-1-Allyl-pentyl)-1,3-dimethoxy-5-((R)-4-methoxymethoxy-2-methyl-butyl)-benzene

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