5-ethylsulfanylcarbonyl-6-(2-hydroxy-ethyl)-2-phenyl-4-propyl-nicotinic acid propyl ester

Base Information

Chemical Name:5-ethylsulfanylcarbonyl-6-(2-hydroxy-ethyl)-2-phenyl-4-propyl-nicotinic acid propyl ester
CAS No.:223679-04-7
Molecular Formula:C₂₃H₂₉NO₄S
Molecular Weight:415.554
Hs Code.:

Synonyms:5-ethylsulfanylcarbonyl-6-(2-hydroxy-ethyl)-2-phenyl-4-propyl-nicotinic acid propyl ester

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Chemical Property of 5-ethylsulfanylcarbonyl-6-(2-hydroxy-ethyl)-2-phenyl-4-propyl-nicotinic acid propyl ester

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Technology Process of 5-ethylsulfanylcarbonyl-6-(2-hydroxy-ethyl)-2-phenyl-4-propyl-nicotinic acid propyl ester

There total 8 articles about 5-ethylsulfanylcarbonyl-6-(2-hydroxy-ethyl)-2-phenyl-4-propyl-nicotinic acid propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 223679-05-8
6-(2-benzyloxy-ethyl)-5-ethylsulfanylcarbonyl-2-phenyl-4-propyl-nicotinic acid propyl ester

: 223679-04-7
5-ethylsulfanylcarbonyl-6-(2-hydroxy-ethyl)-2-phenyl-4-propyl-nicotinic acid propyl ester

Guidance literature:: With boron trifluoride diethyl etherate; ethanethiol; Ambient temperature;
DOI:10.1021/jm980550w

Reference yield:

: 54441-63-3
propyl 3-oxo-3-phenylpropanoate

: 223679-04-7
5-ethylsulfanylcarbonyl-6-(2-hydroxy-ethyl)-2-phenyl-4-propyl-nicotinic acid propyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium acetate / ethanol / 24 h / 80 °C

2: ethanol / 80 °C

3: tetrachloro-1,4-benzoquinone / tetrahydrofuran / Heating

4: 57 percent / BF₃*Et₂O, ethanethiol / Ambient temperature

With ammonium acetate; boron trifluoride diethyl etherate; chloranil; ethanethiol; In tetrahydrofuran; ethanol;
DOI:10.1021/jm980550w

Reference yield:

: 73921-19-4
5-benzoyl-2,2-dimethyl-1,3-dioxane-4,6-dione

: 223679-04-7
5-ethylsulfanylcarbonyl-6-(2-hydroxy-ethyl)-2-phenyl-4-propyl-nicotinic acid propyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / toluene / 24 h / 80 °C

2: ammonium acetate / ethanol / 24 h / 80 °C

3: ethanol / 80 °C

4: tetrachloro-1,4-benzoquinone / tetrahydrofuran / Heating

5: 57 percent / BF₃*Et₂O, ethanethiol / Ambient temperature

With ammonium acetate; boron trifluoride diethyl etherate; chloranil; ethanethiol; In tetrahydrofuran; ethanol; toluene;
DOI:10.1021/jm980550w