[1-(4-Methoxybenzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetic acid

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Chemical Name:[1-(4-Methoxybenzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetic acid
CAS No.:935689-18-2
Molecular Formula:C₁₆H₁₉NO₄S
Molecular Weight:321.397
Hs Code.:

Synonyms:[1-(4-Methoxybenzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetic acid

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Chemical Property of [1-(4-Methoxybenzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetic acid

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Technology Process of [1-(4-Methoxybenzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetic acid

There total 1 articles about [1-(4-Methoxybenzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 732256-60-9
5-Hydroxy-1-(4-methoxybenzyl)-3,4-dimethyl-1,5-dihydropyrrol-2-one

: 68-11-1
mercaptoacetic acid

: 935689-18-2
[1-(4-Methoxybenzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetic acid

Guidance literature:: With camphorsulphonic acid; In dichloromethane; at 0 ℃; for 1.5h;

Reference yield: 56.0%

: 504-29-0
2-aminopyridine

: 935689-18-2
[1-(4-Methoxybenzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetic acid

: 2-[1-(4-Methoxy-benzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-N-pyridin-2-yl-acetamide

Guidance literature:: [1-(4-Methoxybenzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetic acid; With benzotriazol-1-ol; In acetonitrile; for 1h;

2-aminopyridine; With triethylamine; HATU; In acetonitrile; at 20 ℃; for 2h;

Reference yield: 12.0%

: 36052-24-1
methyl 6-aminonicotinoate

: 935689-18-2
[1-(4-Methoxybenzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetic acid

: 6-{2-[1-(4-Methoxy-benzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetylamino}-nicotinic acid methyl ester

Guidance literature:: [1-(4-Methoxybenzyl)-3,4-dimethyl-5-oxo-2,5-dihydro-1H-pyrrol-2-ylsulfanyl]-acetic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 ℃; for 3h;

methyl 6-aminonicotinoate; In dichloromethane; at 0 ℃; for 2.5h;