diethyl 3-amino-4-[{[phenylimino]methylidene}amino]thieno[2,3-b]thiophene-2,5-dicarboxylate

Base Information

• Chemical Name: diethyl 3-amino-4-[{[phenylimino]methylidene}amino]thieno[2,3-b]thiophene-2,5-dicarboxylate
• CAS No.: 1064653-97-9
• Molecular Formula: C₁₉H₁₇N₃O₄S₂
• Molecular Weight: 415.494

Synonyms:diethyl 3-amino-4-[{[phenylimino]methylidene}amino]thieno[2,3-b]thiophene-2,5-dicarboxylate

Chemical Property of diethyl 3-amino-4-[{[phenylimino]methylidene}amino]thieno[2,3-b]thiophene-2,5-dicarboxylate

Chemical Property:

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Technology Process of diethyl 3-amino-4-[{[phenylimino]methylidene}amino]thieno[2,3-b]thiophene-2,5-dicarboxylate

There total 1 articles about diethyl 3-amino-4-[{[phenylimino]methylidene}amino]thieno[2,3-b]thiophene-2,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

diethyl 3-amino-4-[(triphenylphosphoranylidene)amino]thieno[2,3-b]thiophene-2,5-dicarboxylate (1031798-26-1) + phenyl isocyanate (103-71-9) → diethyl 3-amino-4-[{[phenylimino]methylidene}amino]thieno[2,3-b]thiophene-2,5-dicarboxylate (1064653-97-9)

Guidance literature:

In dichloromethane; at 0 - 5 ℃;

DOI:10.1016/j.tet.2008.07.036

Reference yield: 87.0%

diethyl 3-amino-4-[{[phenylimino]methylidene}amino]thieno[2,3-b]thiophene-2,5-dicarboxylate (1064653-97-9) → diethyl 6-(phenylamino)-5H-2,3-dithia-5,7-diazacyclopenta[c,d]indene-1,4-dicarboxylate (1064654-34-7)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃;

DOI:10.1016/j.tet.2008.07.036

Reference yield: 63.0%

diethyl 3-amino-4-[{[phenylimino]methylidene}amino]thieno[2,3-b]thiophene-2,5-dicarboxylate (1064653-97-9) + 3-methyl-phenol (108-39-4) → diethyl 6-(phenylamino)-5H-2,3-dithia-5,7-diazacyclopenta[c,d]indene-1,4-dicarboxylate (1064654-34-7) + 8-amino-7-(ethoxycarbonyl)-2-(3-methylphenoxy)-3-phenyl-thieno[3',2':4,5]thieno[3,2-d]pyrimidin-4(3H)-one (1064654-41-6)

Guidance literature:

With potassium carbonate; In acetonitrile; at 40 - 50 ℃;

DOI:10.1016/j.tet.2008.07.036

upstream raw materials:

diethyl 3-amino-4-[(triphenylphosphoranylidene)amino]thieno[2,3-b]thiophene-2,5-dicarboxylate

phenyl isocyanate

Downstream raw materials:

diethyl 6-(phenylamino)-5H-2,3-dithia-5,7-diazacyclopenta[c,d]indene-1,4-dicarboxylate

8-amino-2-(3,4-dimethylphenoxy)-7-(ethoxycarbonyl)-3-phenyl-thieno[3',2':4,5]thieno[3,2-d]pyrimidin-4(3H)-one

8-amino-2-(2,4-dichloro-6-methylphenoxy)-7-(ethoxycarbonyl)-3-phenyl-thieno[3',2':4,5]thieno[3,2-d]pyrimidin-4(3H)-one

8-amino-7-(ethoxycarbonyl)-2-(3-methylphenoxy)-3-phenyl-thieno[3',2':4,5]thieno[3,2-d]pyrimidin-4(3H)-one

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