m-chlorophenylallyl methyl carbonate

Base Information

Chemical Name:m-chlorophenylallyl methyl carbonate
CAS No.:1239597-21-7
Molecular Formula:C₁₁H₁₁ClO₃
Molecular Weight:226.66
Hs Code.:

Synonyms:m-chlorophenylallyl methyl carbonate

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Chemical Property of m-chlorophenylallyl methyl carbonate

Chemical Property:

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Technology Process of m-chlorophenylallyl methyl carbonate

There total 2 articles about m-chlorophenylallyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1504-67-2
3-(3-chlorophenyl)prop-2-en-1-ol

: 79-22-1
methyl chloroformate

: 1239597-21-7
m-chlorophenylallyl methyl carbonate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; Reflux;
DOI:10.1039/c8cc07249c

Reference yield:

: 56578-37-1,770-23-0
3-(3-chlorophenyl)acrylaldehyde

: 1239597-21-7
m-chlorophenylallyl methyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 2 h / 0 - 20 °C / Schlenk technique

2: pyridine / dichloromethane / 0 - 20 °C / Schlenk technique

With pyridine; sodium tetrahydroborate; In methanol; dichloromethane;
DOI:10.1021/jacs.1c09148

Reference yield: 97.0%

: 1239597-21-7
m-chlorophenylallyl methyl carbonate

: anthracen-9(10H)-one

: C₂₃H₁₉ClO

Guidance literature:: With propylamine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; N-benzhydryl-N-phenyldinaphthophosphoramidite; lithium tert-butoxide; In dichloromethane; at 20 ℃; for 10h; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.cclet.2016.02.017