N-cyclobutanoyl-N'-[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbonyl]-hydrazine

Base Information

• Chemical Name: N-cyclobutanoyl-N'-[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbonyl]-hydrazine
• CAS No.: 1020796-12-6
• Molecular Formula: C₂₂H₁₉Cl₃N₄O₂
• Molecular Weight: 477.777

Synonyms:N-cyclobutanoyl-N'-[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbonyl]-hydrazine

Chemical Property of N-cyclobutanoyl-N'-[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbonyl]-hydrazine

Chemical Property:

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Technology Process of N-cyclobutanoyl-N'-[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbonyl]-hydrazine

There total 2 articles about N-cyclobutanoyl-N'-[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbonyl]-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclobutanecarboxylic acid hydrazide (98069-56-8) + rimonabant acid (162758-35-2) → N-cyclobutanoyl-N'-[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbonyl]-hydrazine (1020796-12-6)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; at 20 ℃; Inert atmosphere;

DOI:10.1021/jm800843r

Reference yield:

Cyclobutanecarboxylic acid (3721-95-7) + 5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbohydrazide (443141-90-0) → N-cyclobutanoyl-N'-[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbonyl]-hydrazine (1020796-12-6)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; at 20 ℃; Inert atmosphere;

DOI:10.1021/jm800843r

Reference yield: 43.0%

N-cyclobutanoyl-N'-[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbonyl]-hydrazine (1020796-12-6) → 2-(5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazol-3-yl)-5-cyclobutyl-1,3,4-thiadiazole

Guidance literature:

With Lawessons reagent; In 1,4-dioxane; at 180 ℃; for 0.5h; Microwave irradiation;

upstream raw materials:

Cyclobutanecarboxylic acid

5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbohydrazide

cyclobutanecarboxylic acid hydrazide

rimonabant acid

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