(2S,3R)-2-(benzyloxycarbonylmethylamino)-3-(4-benzyloxy-3-hydroxyphenyl)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

Base Information

Chemical Name:(2S,3R)-2-(benzyloxycarbonylmethylamino)-3-(4-benzyloxy-3-hydroxyphenyl)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester
CAS No.:1013210-32-6
Molecular Formula:C₃₉H₄₇NO₈Si
Molecular Weight:685.89
Hs Code.:

(2S,3R)-2-(benzyloxycarbonylmethylamino)-3-(4-benzyloxy-3-hydroxyphenyl)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

Synonyms:(2S,3R)-2-(benzyloxycarbonylmethylamino)-3-(4-benzyloxy-3-hydroxyphenyl)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

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Chemical Property of (2S,3R)-2-(benzyloxycarbonylmethylamino)-3-(4-benzyloxy-3-hydroxyphenyl)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

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Technology Process of (2S,3R)-2-(benzyloxycarbonylmethylamino)-3-(4-benzyloxy-3-hydroxyphenyl)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

There total 1 articles about (2S,3R)-2-(benzyloxycarbonylmethylamino)-3-(4-benzyloxy-3-hydroxyphenyl)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1013210-73-5
(2S,3R)-2-(benzyloxycarbonylmethylamino)-3-(4-benzyloxy-3-hydroxyphenyl)-3-(tert-butyldimethylsilanyloxy)propionic acid

: 2746-25-0
p-Methoxybenzyl bromide

: 1013210-32-6
(2S,3R)-2-(benzyloxycarbonylmethylamino)-3-(4-benzyloxy-3-hydroxyphenyl)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; for 16h;
DOI:10.1021/ja710363p

Reference yield: 96.0%

: 1013210-32-6
(2S,3R)-2-(benzyloxycarbonylmethylamino)-3-(4-benzyloxy-3-hydroxyphenyl)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

: 1838-94-4
isoprene epoxide

: (2S,3R)-2-[[(benzyloxycarbonyl)methyl]amino]-3-[4-(benzyloxy)-3-[(1S)-1-(hydroxymethyl)-1-(methylallyl)oxy]phenyl]-3-[(tertbutyldimethylsilanyl)oxy]propionic acid 4-methoxybenzyl ester

: (2S,3R)-2-[[(benzyloxycarbonyl)methyl]amino]-3-[4-(benzyloxy)-3-[(1R)-1-(hydroxymethyl)-1-(methylallyl)oxy]phenyl]-3-[(tertbutyldimethylsilanyl)oxy]propionic acid 4-methoxybenzyl ester

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In dichloromethane; for 18h; Inert atmosphere;
DOI:10.1021/acs.joc.5b01519

Reference yield: 78.0%

: 1013210-32-6
(2S,3R)-2-(benzyloxycarbonylmethylamino)-3-(4-benzyloxy-3-hydroxyphenyl)-3-(tert-butyldimethylsilanyloxy)propionic acid 4-methoxybenzyl ester

: 1297295-80-7
C₂₁H₁₉N₃O₇S

: 1297295-85-2
C₆₀H₆₆N₄O₁₅SSi

Guidance literature:: With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; In toluene; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.tetlet.2010.11.165