1,5-bis(2,2-bis((3,7-dimethyloctyl)oxy)ethyl)-3,7-bis(4-bromophenyl)pyrrolo[2,3-f]indole-2,6(1H,5H)-dione

Base Information

Chemical Name:1,5-bis(2,2-bis((3,7-dimethyloctyl)oxy)ethyl)-3,7-bis(4-bromophenyl)pyrrolo[2,3-f]indole-2,6(1H,5H)-dione
CAS No.:1403769-60-7
Molecular Formula:C₆₆H₁₀₀Br₂N₂O₆
Molecular Weight:1177.34
Hs Code.:

Synonyms:1,5-bis(2,2-bis((3,7-dimethyloctyl)oxy)ethyl)-3,7-bis(4-bromophenyl)pyrrolo[2,3-f]indole-2,6(1H,5H)-dione

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Chemical Property of 1,5-bis(2,2-bis((3,7-dimethyloctyl)oxy)ethyl)-3,7-bis(4-bromophenyl)pyrrolo[2,3-f]indole-2,6(1H,5H)-dione

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Technology Process of 1,5-bis(2,2-bis((3,7-dimethyloctyl)oxy)ethyl)-3,7-bis(4-bromophenyl)pyrrolo[2,3-f]indole-2,6(1H,5H)-dione

There total 5 articles about 1,5-bis(2,2-bis((3,7-dimethyloctyl)oxy)ethyl)-3,7-bis(4-bromophenyl)pyrrolo[2,3-f]indole-2,6(1H,5H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.7%

: 1335131-35-5
3,7-di(4-bromophenyl)-2,6-dioxo-1,2,5,6-tetrahydrobenzo[1,2-b:4,5-b']dipyrrole

: 1393357-66-8
2,2-bis((3,7-dimethyloctyl)oxy)ethyl bromide

: 1403769-60-7
1,5-bis(2,2-bis((3,7-dimethyloctyl)oxy)ethyl)-3,7-bis(4-bromophenyl)pyrrolo[2,3-f]indole-2,6(1H,5H)-dione

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 130 ℃;
DOI:10.1039/c2jm34867e

Reference yield:

: 106-21-8,59204-02-3
tetrahydrogeraniol

: 1403769-60-7
1,5-bis(2,2-bis((3,7-dimethyloctyl)oxy)ethyl)-3,7-bis(4-bromophenyl)pyrrolo[2,3-f]indole-2,6(1H,5H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonic acid / 120 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 130 °C

With methanesulfonic acid; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/c2jm34867e

Reference yield:

: 6940-50-7
4-bromo-DL-mandelic acid

: 1403769-60-7
1,5-bis(2,2-bis((3,7-dimethyloctyl)oxy)ethyl)-3,7-bis(4-bromophenyl)pyrrolo[2,3-f]indole-2,6(1H,5H)-dione

Guidance literature:: Multi-step reaction with 4 steps

1: chlorobenzene / 130 °C

2: sulfuric acid

3: sodium hydroxide; dihydrogen peroxide / water; ethanol / 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 130 °C

With sulfuric acid; dihydrogen peroxide; potassium carbonate; sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1039/c2jm34867e