methyl 4-O-benzoyl-2,3-di-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 4-O-benzoyl-2,3-di-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside
CAS No.:1214746-48-1
Molecular Formula:C₂₆H₄₆O₇Si₂
Molecular Weight:526.818
Hs Code.:

Synonyms:methyl 4-O-benzoyl-2,3-di-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-O-benzoyl-2,3-di-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

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Technology Process of methyl 4-O-benzoyl-2,3-di-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

There total 2 articles about methyl 4-O-benzoyl-2,3-di-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1214746-46-9
(((2R,4αR,6S,7R,8S,8αR)-6-methoxy-2-phenylhexahydropyrano[3,2-d][1,3]dioxine-7,8-diyl)bis(oxy))bis(tert-butyldimethylsilane)

: 1214746-48-1
methyl 4-O-benzoyl-2,3-di-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

Guidance literature:: With 3,3-dimethyldioxirane; In acetone; at 5 ℃; for 96h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo9026098

Reference yield:

: 1214746-46-9
(((2R,4αR,6S,7R,8S,8αR)-6-methoxy-2-phenylhexahydropyrano[3,2-d][1,3]dioxine-7,8-diyl)bis(oxy))bis(tert-butyldimethylsilane)

: 1214746-48-1
methyl 4-O-benzoyl-2,3-di-O-(tert-butyldimethylsilyl)-α-D-glucopyranoside

: C₂₆H₄₆O₇Si₂

Guidance literature:: With aluminum oxide; tetrabutylammomium bromide; periodic acid; In dichloromethane; at 20 ℃; for 1.5h; Overall yield = 98 %; regioselective reaction;
DOI:10.1055/s-0033-1340056