Acetanilide, 2-cyano-2-(triphenylphosphoranylidene)-

Base Information

Chemical Name:Acetanilide, 2-cyano-2-(triphenylphosphoranylidene)-
CAS No.:73623-35-5
Molecular Formula:C27H21N2OP
Molecular Weight:420.45
Hs Code.:
DSSTox Substance ID:DTXSID60223839
Nikkaji Number:J73.563I
Wikidata:Q83102333

Synonyms:BRN 3475303;2-Cyano-2-(triphenylphosphoranylidene)acetanilide;Acetanilide, 2-cyano-2-(triphenylphosphoranylidene)-;73623-35-5;4-16-00-00978 (Beilstein Handbook Reference);C27H21N2OP;DTXSID60223839;C27-H21-N2-O-P;Acetamide, 2-cyano-N-phenyl-2-(triphenylphosphoranylidene)-

Suppliers and Price of Acetanilide, 2-cyano-2-(triphenylphosphoranylidene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Acetanilide, 2-cyano-2-(triphenylphosphoranylidene)-

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.24g/cm³
XLogP3:5.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:420.13915030
Heavy Atom Count:31
Complexity:644

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC(=O)C(=P(C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4)C#N

Technology Process of Acetanilide, 2-cyano-2-(triphenylphosphoranylidene)-

There total 4 articles about Acetanilide, 2-cyano-2-(triphenylphosphoranylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 103-71-9
phenyl isocyanate

: 16640-68-9
cyanomethylene triphenylphosphorane

: 73623-35-5
[(cyano)(phenylcarbamoyl)methylene]triphenylphosphorane

Guidance literature:: In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/kin.20170

Reference yield:

: 4336-70-3
(cyanomethyl)triphenylphosphonium chloride

: 73623-35-5
[(cyano)(phenylcarbamoyl)methylene]triphenylphosphorane

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / Et₃N / CH₂Cl₂ / 0.5 h

2: 90 percent / CH₂Cl₂ / 2 h / 20 °C

With triethylamine; In dichloromethane;
DOI:10.1002/kin.20170

Reference yield:

: 603-35-0
triphenylphosphine

: 73623-35-5
[(cyano)(phenylcarbamoyl)methylene]triphenylphosphorane

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / ethyl acetate / 1.5 h / Heating

2: 79 percent / Et₃N / CH₂Cl₂ / 0.5 h

3: 90 percent / CH₂Cl₂ / 2 h / 20 °C

With triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1002/kin.20170