benzyloxycarbonylmethylsulfonyl chloride

Base Information

• Chemical Name: benzyloxycarbonylmethylsulfonyl chloride
• CAS No.: 159215-13-1
• Molecular Formula: C₉H₉ClO₄S
• Molecular Weight: 248.687

Synonyms:benzyloxycarbonylmethylsulfonyl chloride

Chemical Property of benzyloxycarbonylmethylsulfonyl chloride

Chemical Property:

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Technology Process of benzyloxycarbonylmethylsulfonyl chloride

There total 1 articles about benzyloxycarbonylmethylsulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chlorosulfonylacetyl chloride (4025-77-8) + benzyl alcohol (100-51-6,185532-71-2) → benzyloxycarbonylmethylsulfonyl chloride (159215-13-1)

Guidance literature:

In benzene; at 0 ℃; for 1h; Yield given;

DOI:10.7164/antibiotics.47.1041

Reference yield: 61.8%

benzyl (2S,5R,6R)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate (3956-31-8,49626-54-2,64519-71-7) + benzyloxycarbonylmethylsulfonyl chloride (159215-13-1) → benzyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate (159215-16-4)

Guidance literature:

With triethylamine; In dichloromethane; for 0.5h; Ambient temperature;

DOI:10.7164/antibiotics.47.1041

Reference yield: 50.0%

benzyloxycarbonylmethylsulfonyl chloride (159215-13-1) + 1-(4-aminophenyl)piperidin-4-one hydrochloride → [4-(4-oxopiperidin-1-yl)phenylsulfamoyl]acetic acid benzyl ester (373359-63-8)

Guidance literature:

With triethylamine; In 1,4-dioxane; for 24h;

DOI:10.1016/S0968-0896(01)00114-6

upstream raw materials:

chlorosulfonylacetyl chloride

benzyl alcohol

Downstream raw materials:

benzyl 6-β-<(p-nitrobenzyloxycarbonyl)methylsulfonamido>penicillinate

methoxymethyl 6-β-<(benzyloxycarbonyl)methylsulfonamido>penicillinate

{butyl[4-(4-oxopiperidin-1-yl)phenyl]sulfamoyl}acetic acid benzyl ester

[4-(4-oxopiperidin-1-yl)phenylsulfamoyl]acetic acid benzyl ester

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