C₃₄H₃₆INO₆Si

Base Information

Chemical Name:C₃₄H₃₆INO₆Si
CAS No.:1331965-90-2
Molecular Formula:C₃₄H₃₆INO₆Si
Molecular Weight:709.653
Hs Code.:

C<sub>34</sub>H<sub>36</sub>INO<sub>6</sub>Si

Synonyms:C₃₄H₃₆INO₆Si

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Chemical Property of C₃₄H₃₆INO₆Si

Chemical Property:

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Technology Process of C₃₄H₃₆INO₆Si

There total 7 articles about C₃₄H₃₆INO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1331965-86-6
N-(2,4-bis(benzyloxy)phenyl)-6-iodobenzo[d][1,3]dioxole-5-carboxamide

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 1331965-90-2
C₃₄H₃₆INO₆Si

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1007/s12272-011-0703-1

Reference yield:

: C₂₃H₂₃NO₄

: 1331965-90-2
C₃₄H₃₆INO₆Si

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol / 18 h / Reflux; Inert atmosphere

2: triethylamine / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

With sodium hydride; triethylamine; potassium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1007/s12272-011-0703-1

Reference yield:

: 13246-46-3
2,4-dibenzyloxybenzaldehyde

: 1331965-90-2
C₃₄H₃₆INO₆Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; acetonitrile; tert-butyl alcohol / 0.17 h / 20 °C / Inert atmosphere

2.1: diphenyl phosphoryl azide; triethylamine / 1,4-dioxane / 0.5 h / 20 °C / Inert atmosphere

2.2: 2 h / Reflux; Inert atmosphere

3.1: potassium hydroxide / ethanol / 18 h / Reflux; Inert atmosphere

4.1: triethylamine / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; sodium hydride; triethylamine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; acetonitrile; mineral oil; tert-butyl alcohol; 2.1: Curtius rearrangement / 2.2: Curtius rearrangement;
DOI:10.1007/s12272-011-0703-1