3,7-bis(4-nitrophenyl)-15-(triisopropylsilylethynyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrin Ni(II)

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Chemical Name:3,7-bis(4-nitrophenyl)-15-(triisopropylsilylethynyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrin Ni(II)
CAS No.:1573176-65-4
Molecular Formula:C₇₁H₇₈N₆NiO₄Si
Molecular Weight:1166.21
Hs Code.:

Synonyms:3,7-bis(4-nitrophenyl)-15-(triisopropylsilylethynyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrin Ni(II)

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Chemical Property of 3,7-bis(4-nitrophenyl)-15-(triisopropylsilylethynyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrin Ni(II)

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Technology Process of 3,7-bis(4-nitrophenyl)-15-(triisopropylsilylethynyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrin Ni(II)

There total 1 articles about 3,7-bis(4-nitrophenyl)-15-(triisopropylsilylethynyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrin Ni(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1573176-61-0
C₇₁H₉₄B₂N₄NiO₄Si

: 586-78-7
para-nitrophenyl bromide

: 1573176-65-4
3,7-bis(4-nitrophenyl)-15-(triisopropylsilylethynyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrin Ni(II)

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; In water; N,N-dimethyl-formamide; toluene; at 100 ℃; for 5h; Schlenk technique; Inert atmosphere;
DOI:10.1021/ol500569b

Reference yield: 53.0%

: 1573176-65-4
3,7-bis(4-nitrophenyl)-15-(triisopropylsilylethynyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrin Ni(II)

: 1573176-67-6
3,7-bis(4-nitrophenyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrin Ni(II)

Guidance literature:: 3,7-bis(4-nitrophenyl)-15-(triisopropylsilylethynyl)-10,20-bis(3,5-di-tert-butylphenyl)porphyrin Ni(II); With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -50 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;

With para-dodecylbenzenesulfonic acid; In water; 1,2-dichloro-ethane; at 95 ℃; for 24h;
DOI:10.1021/ol500569b