1-chloro-2,3,6-trideoxy-4-O-(p-nitrobenzoyl)-3-(trifluoroacetamido)-α-L-lyxo-hexopyranose

Base Information

• Chemical Name: 1-chloro-2,3,6-trideoxy-4-O-(p-nitrobenzoyl)-3-(trifluoroacetamido)-α-L-lyxo-hexopyranose
• CAS No.: 78548-38-6
• Molecular Formula: C₁₅H₁₄ClF₃N₂O₆
• Molecular Weight: 410.734

Synonyms:1-chloro-2,3,6-trideoxy-4-O-(p-nitrobenzoyl)-3-(trifluoroacetamido)-α-L-lyxo-hexopyranose

Chemical Property of 1-chloro-2,3,6-trideoxy-4-O-(p-nitrobenzoyl)-3-(trifluoroacetamido)-α-L-lyxo-hexopyranose

Chemical Property:

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Technology Process of 1-chloro-2,3,6-trideoxy-4-O-(p-nitrobenzoyl)-3-(trifluoroacetamido)-α-L-lyxo-hexopyranose

There total 2 articles about 1-chloro-2,3,6-trideoxy-4-O-(p-nitrobenzoyl)-3-(trifluoroacetamido)-α-L-lyxo-hexopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

→ 1-chloro-2,3,6-trideoxy-4-O-(p-nitrobenzoyl)-3-(trifluoroacetamido)-α-L-lyxo-hexopyranose (78548-38-6)

Guidance literature:

With hydrogenchloride; In dichloromethane; at 25 ℃; for 0.166667h;

DOI:10.1021/jo00186a034

Reference yield:

→ 4-Nitro-benzoic acid (2S,3S,4S,6R)-6-chloro-2-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-3-yl ester (59044-90-5,62414-05-5,63700-25-4,67463-63-2,70629-82-2,78548-38-6,81844-79-3,128572-89-4)

Guidance literature:

HCl, 1,4-Di-O-p-nitrobenzoyl-3-N-trifluoracetyldaunosamin, p-Nitrobenzoesaeure;

DOI:10.1021/jm00201a009

Reference yield:

cis-2-Acetyl-2,3-dihydro-2,3-dihydroxy-1H-cyclopentanthracene-4,11-dione (90269-95-7) + 1-chloro-2,3,6-trideoxy-4-O-(p-nitrobenzoyl)-3-(trifluoroacetamido)-α-L-lyxo-hexopyranose (78548-38-6) → 4-Nitro-benzoic acid (2S,3S,4S,6S)-6-((1R,2S)-2-acetyl-2-hydroxy-4,11-dioxo-2,3,4,11-tetrahydro-1H-cyclopenta[b]anthracen-1-yloxy)-2-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-3-yl ester (90270-00-1,90364-55-9) + 4-Nitro-benzoic acid (2S,3S,4S,6S)-6-((1S,2R)-2-acetyl-2-hydroxy-4,11-dioxo-2,3,4,11-tetrahydro-1H-cyclopenta[b]anthracen-1-yloxy)-2-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-3-yl ester (90270-00-1,90364-55-9)

Guidance literature:

With silver trifluoromethanesulfonate; calcium carbonate; In tetrahydrofuran; dichloromethane; at 25 ℃; for 0.25h; Yield given. Yields of byproduct given;

DOI:10.1021/jo00186a034

Downstream raw materials:

4-Nitro-benzoic acid (2S,3S,4S,6S)-6-((1R,2S)-2-acetyl-2-hydroxy-4,11-dioxo-2,3,4,11-tetrahydro-1H-cyclopenta[b]anthracen-1-yloxy)-2-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-3-yl ester

4-Nitro-benzoic acid (2S,3S,4S,6S)-6-((1S,2R)-2-acetyl-2-hydroxy-4,11-dioxo-2,3,4,11-tetrahydro-1H-cyclopenta[b]anthracen-1-yloxy)-2-methyl-4-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-3-yl ester

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