1-<4-Chlorphenyl-amino>-4-brom-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien

Base Information

• Chemical Name: 1-<4-Chlorphenyl-amino>-4-brom-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien
• CAS No.: 109599-43-1
• Molecular Formula: C₁₉H₁₃BrCl₂N₂
• Molecular Weight: 420.136

Synonyms:1-<4-Chlorphenyl-amino>-4-brom-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien

Chemical Property of 1-<4-Chlorphenyl-amino>-4-brom-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien

Chemical Property:

Purity/Quality:

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Technology Process of 1-<4-Chlorphenyl-amino>-4-brom-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien

There total 5 articles about 1-<4-Chlorphenyl-amino>-4-brom-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,5,6,6-tetrafluoro-cyclohepta-1,3-diene (2267-32-5) → 1-<4-Chlorphenyl-amino>-4-brom-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien (109599-43-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Br₂ / Irradiation

2: Et₃N

With bromine; triethylamine;

DOI:10.1021/ja01475a031

Reference yield:

1-<4-Chlorphenyl-amino>-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien (6450-19-7) → 1-<4-Chlorphenyl-amino>-4-brom-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien (109599-43-1)

Guidance literature:

With bromine;

DOI:10.1021/ja01475a031

Reference yield:

4-chloro-aniline (106-47-8) → 1-<4-Chlorphenyl-amino>-4-brom-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien (109599-43-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N

2: Br₂

With bromine; triethylamine;

DOI:10.1021/ja01475a031

upstream raw materials:

1-<4-Chlorphenyl-amino>-7-<4-chlorphenyl-imino>-1,3,5-cycloheptatrien

3,4-Dibrom-6,6,7,7-tetrafluor-cyclohepten-⁽¹⁾

4-chloro-aniline

5,5,6,6-tetrafluoro-cyclohepta-1,3-diene

Downstream raw materials:

{Ni(ClC₆H₄NC₇H₄BrNC₆H₄Cl)2}

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