4-[3-(Naphthalene-2-sulfonylamino)-4-oxo-4-piperidin-1-yl-butyl]-benzamidine; hydriodide

Base Information

Chemical Name:4-[3-(Naphthalene-2-sulfonylamino)-4-oxo-4-piperidin-1-yl-butyl]-benzamidine; hydriodide
CAS No.:82099-40-9
Molecular Formula:C₂₆H₃₀N₄O₃S*HI
Molecular Weight:606.528
Hs Code.:

Synonyms:4-[3-(Naphthalene-2-sulfonylamino)-4-oxo-4-piperidin-1-yl-butyl]-benzamidine; hydriodide

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Chemical Property of 4-[3-(Naphthalene-2-sulfonylamino)-4-oxo-4-piperidin-1-yl-butyl]-benzamidine; hydriodide

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Technology Process of 4-[3-(Naphthalene-2-sulfonylamino)-4-oxo-4-piperidin-1-yl-butyl]-benzamidine; hydriodide

There total 9 articles about 4-[3-(Naphthalene-2-sulfonylamino)-4-oxo-4-piperidin-1-yl-butyl]-benzamidine; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 82099-19-2
4-[3-(Naphthalene-2-sulfonylamino)-4-oxo-4-piperidin-1-yl-butyl]-thiobenzimidic acid methyl ester; hydriodide

: 82099-40-9
4-[3-(Naphthalene-2-sulfonylamino)-4-oxo-4-piperidin-1-yl-butyl]-benzamidine; hydriodide

Guidance literature:: With ammonium acetate; In ethanol; at 60 - 70 ℃; for 3h;

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 82099-40-9
4-[3-(Naphthalene-2-sulfonylamino)-4-oxo-4-piperidin-1-yl-butyl]-benzamidine; hydriodide

Guidance literature:: Multi-step reaction with 9 steps

1: 70 percent / H₂ / Raney-nickel / methanol / Ambient temperature

2: 1.) NaNO₂/conc. HCl; 2.) CuCN/NaCN / 1.) H₂O, 0-5 deg C; 2.) benzene, 0-5 deg C, 30 min; room temp., 4 h

3: 63 percent / PBr₃ / CHCl₃ / 1.5 h / Heating

4: 1.) KI; 2.) Na / 1.) EtOH, reflux; 2.) EtOH, reflux, 5 h

6: 95 percent / benzene / Ambient temperature

7: 93.5 percent / H₂S (gas), TEA / pyridine / Ambient temperature

8: 86 percent / acetone / Ambient temperature

9: 72 percent / ammonium acetate / ethanol / 3 h / 60 - 70 °C

With ammonium acetate; hydrogenchloride; TEA; hydrogen sulfide; sodium cyanide; hydrogen; sodium; phosphorus tribromide; potassium iodide; sodium nitrite; nickel; In pyridine; methanol; ethanol; chloroform; acetone; benzene;

Reference yield:

: 72054-56-9
4-(2-bromoethyl)benzonitrile

: 82099-40-9
4-[3-(Naphthalene-2-sulfonylamino)-4-oxo-4-piperidin-1-yl-butyl]-benzamidine; hydriodide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) KI; 2.) Na / 1.) EtOH, reflux; 2.) EtOH, reflux, 5 h

3: 95 percent / benzene / Ambient temperature

4: 93.5 percent / H₂S (gas), TEA / pyridine / Ambient temperature

5: 86 percent / acetone / Ambient temperature

6: 72 percent / ammonium acetate / ethanol / 3 h / 60 - 70 °C

With ammonium acetate; TEA; hydrogen sulfide; sodium; potassium iodide; In pyridine; ethanol; acetone; benzene;