5,17,29-tri-tert-butyl-38,40,42-trimethoxy-37,39,41-tri-n-octyloxy-11,23,35-tris-(N'-phenylureyl)-calix[6]arene

Base Information

Chemical Name:5,17,29-tri-tert-butyl-38,40,42-trimethoxy-37,39,41-tri-n-octyloxy-11,23,35-tris-(N'-phenylureyl)-calix[6]arene
CAS No.:259886-66-3
Molecular Formula:C₁₀₂H₁₃₂N₆O₉
Molecular Weight:1586.2
Hs Code.:

Synonyms:5,17,29-tri-tert-butyl-38,40,42-trimethoxy-37,39,41-tri-n-octyloxy-11,23,35-tris-(N'-phenylureyl)-calix[6]arene

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Chemical Property of 5,17,29-tri-tert-butyl-38,40,42-trimethoxy-37,39,41-tri-n-octyloxy-11,23,35-tris-(N'-phenylureyl)-calix[6]arene

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Technology Process of 5,17,29-tri-tert-butyl-38,40,42-trimethoxy-37,39,41-tri-n-octyloxy-11,23,35-tris-(N'-phenylureyl)-calix[6]arene

There total 1 articles about 5,17,29-tri-tert-butyl-38,40,42-trimethoxy-37,39,41-tri-n-octyloxy-11,23,35-tris-(N'-phenylureyl)-calix[6]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 103-71-9
phenyl isocyanate

: 259886-63-0
5,17,29-triamino-11,23,35-tris(1,1-dimethylethyl)-37,39,41-trimethoxy-38,40,42-tri-n-octyloxycalix[6]arene

: 259886-66-3
5,17,29-tri-tert-butyl-38,40,42-trimethoxy-37,39,41-tri-n-octyloxy-11,23,35-tris-(N'-phenylureyl)-calix[6]arene

Guidance literature:: In dichloromethane; at 25 ℃; for 5h;
DOI:10.1002/(SICI)1521-3765(20000103)6:1<73::AID-CHEM73>3.0.CO;2-#

Reference yield: 69.0%

: 1-(12-{11-[(3,5-di-tert-butylphenoxy)undecyl](tert-butoxycarbonyl)amino}dodecyl)-4,4’-bipyridin-1-ium bromide

: 532438-33-8
6-bromohexyl diphenylacetate

: 76-05-1
trifluoroacetic acid

: 259886-66-3
5,17,29-tri-tert-butyl-38,40,42-trimethoxy-37,39,41-tri-n-octyloxy-11,23,35-tris-(N'-phenylureyl)-calix[6]arene

: C₆₇H₉₉N₃O₃⁽²⁺⁾*2C₇H₇O₃S^(1-)*C₂HF₃O₂*C₁₀₂H₁₃₂N₆O₉

Guidance literature:: 1-(12-{11-[(3,5-di-tert-butylphenoxy)undecyl](tert-butoxycarbonyl)amino}dodecyl)-4,4’-bipyridin-1-ium bromide; 6-bromohexyl diphenylacetate; 5,17,29-tri-tert-butyl-38,40,42-trimethoxy-37,39,41-tri-n-octyloxy-11,23,35-tris-(N'-phenylureyl)-calix[6]arene; In toluene; at 110 ℃; for 48h;

trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/chem.201800496

Reference yield: 58.0%

: 1-(6-{6-[(3,5-di-tert-butylphenoxy)hexyl](tert-butoxycarbonyl)-amino}hexyl)-4,4’-bipyridin-1-ium bromide

: 532438-33-8
6-bromohexyl diphenylacetate

: 76-05-1
trifluoroacetic acid

: 259886-66-3
5,17,29-tri-tert-butyl-38,40,42-trimethoxy-37,39,41-tri-n-octyloxy-11,23,35-tris-(N'-phenylureyl)-calix[6]arene

: C₅₆H₇₇N₃O₃⁽²⁺⁾*2C₇H₇O₃S^(1-)*C₂HF₃O₂*C₁₀₂H₁₃₂N₆O₉

Guidance literature:: 1-(6-{6-[(3,5-di-tert-butylphenoxy)hexyl](tert-butoxycarbonyl)-amino}hexyl)-4,4’-bipyridin-1-ium bromide; 6-bromohexyl diphenylacetate; 5,17,29-tri-tert-butyl-38,40,42-trimethoxy-37,39,41-tri-n-octyloxy-11,23,35-tris-(N'-phenylureyl)-calix[6]arene; In toluene; at 110 ℃; for 48h;

trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/chem.201800496