Technology Process of C14H15N3O3
There total 6 articles about C14H15N3O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C14H14N2O4;
With
4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine;
In
dichloromethane;
at 20 ℃;
for 2.5h;
With
ammonia;
for 2h;
DOI:10.1039/c2cc18012j
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 2 h / 20 °C
2.1: 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine / dichloromethane / 2.5 h / 20 °C
2.2: 2 h
With
4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; lithium hydroxide monohydrate;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c2cc18012j
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: Rhodococcus erythropolis AJ270; water / 12 h / 30 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction
2.1: sodium hydrogencarbonate / ethanol; water / 20 °C
3.1: thionyl chloride / 4 h / 20 °C
4.1: thionyl chloride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C
5.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 2 h / 20 °C
6.1: 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine / dichloromethane / 2.5 h / 20 °C
6.2: 2 h
With
4-methyl-morpholine; thionyl chloride; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; lithium hydroxide monohydrate; Rhodococcus erythropolis AJ270; water; sodium hydrogencarbonate;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c2cc18012j
