ethyl 5-[2-({[1-[4-(di-tert-butylfluorosilyl)benzyl]-1H-1,2,3-triazole-4-yl]methyl}(methyl)amino)ethoxy]-1H-indole-2-carboxylate

Base Information

Chemical Name:ethyl 5-[2-({[1-[4-(di-tert-butylfluorosilyl)benzyl]-1H-1,2,3-triazole-4-yl]methyl}(methyl)amino)ethoxy]-1H-indole-2-carboxylate
CAS No.:1333414-93-9
Molecular Formula:C₃₂H₄₄FN₅O₃Si
Molecular Weight:593.817
Hs Code.:

Synonyms:ethyl 5-[2-({[1-[4-(di-tert-butylfluorosilyl)benzyl]-1H-1,2,3-triazole-4-yl]methyl}(methyl)amino)ethoxy]-1H-indole-2-carboxylate

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Chemical Property of ethyl 5-[2-({[1-[4-(di-tert-butylfluorosilyl)benzyl]-1H-1,2,3-triazole-4-yl]methyl}(methyl)amino)ethoxy]-1H-indole-2-carboxylate

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Technology Process of ethyl 5-[2-({[1-[4-(di-tert-butylfluorosilyl)benzyl]-1H-1,2,3-triazole-4-yl]methyl}(methyl)amino)ethoxy]-1H-indole-2-carboxylate

There total 2 articles about ethyl 5-[2-({[1-[4-(di-tert-butylfluorosilyl)benzyl]-1H-1,2,3-triazole-4-yl]methyl}(methyl)amino)ethoxy]-1H-indole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1333414-88-2
4-(di-tert-butylfluorosilyl)benzylazide

: 1333414-89-3
C₁₇H₂₀N₂O₃

: 1333414-93-9
ethyl 5-[2-({[1-[4-(di-tert-butylfluorosilyl)benzyl]-1H-1,2,3-triazole-4-yl]methyl}(methyl)amino)ethoxy]-1H-indole-2-carboxylate

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 0.333333h; chemoselective reaction; Inert atmosphere;
DOI:10.1055/s-0030-1260942

Reference yield:

: 1146956-36-6
4-(di-tert-butylfluorosilanyl)benzyl alcohol

: 1333414-93-9
ethyl 5-[2-({[1-[4-(di-tert-butylfluorosilyl)benzyl]-1H-1,2,3-triazole-4-yl]methyl}(methyl)amino)ethoxy]-1H-indole-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 13 h / 50 °C / Inert atmosphere

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 0.33 h / 20 °C / Inert atmosphere

With copper(ll) sulfate pentahydrate; diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium L-ascorbate; In water; toluene; tert-butyl alcohol;
DOI:10.1055/s-0030-1260942