4,6-O-diacetyl-3-O-((R)-phenylsulfonylethyl-propion-2-yl)-N-acetyl-α-D-glucosamine

Base Information

Chemical Name:4,6-O-diacetyl-3-O-((R)-phenylsulfonylethyl-propion-2-yl)-N-acetyl-α-D-glucosamine
CAS No.:359773-59-4
Molecular Formula:C₂₃H₃₁NO₁₂S
Molecular Weight:545.565
Hs Code.:

Synonyms:4,6-O-diacetyl-3-O-((R)-phenylsulfonylethyl-propion-2-yl)-N-acetyl-α-D-glucosamine

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Chemical Property of 4,6-O-diacetyl-3-O-((R)-phenylsulfonylethyl-propion-2-yl)-N-acetyl-α-D-glucosamine

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Technology Process of 4,6-O-diacetyl-3-O-((R)-phenylsulfonylethyl-propion-2-yl)-N-acetyl-α-D-glucosamine

There total 9 articles about 4,6-O-diacetyl-3-O-((R)-phenylsulfonylethyl-propion-2-yl)-N-acetyl-α-D-glucosamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 202464-71-9
1-O-benzyl-4,6-O-diacetyl-3-O-((R)-phenylsulfonylethyl-propion-2-yl)-N-acetyl-α-D-glucosamine

: 359773-59-4
4,6-O-diacetyl-3-O-((R)-phenylsulfonylethyl-propion-2-yl)-N-acetyl-α-D-glucosamine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 5h; under 760.051 Torr;
DOI:10.1021/ja302099u

Reference yield:

: 202464-70-8
benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(D-1-{[2-(phenylsulfonyl)ethoxy]carbonyl}ethyl)-α-D-glucopyranoside

: 359773-59-4
4,6-O-diacetyl-3-O-((R)-phenylsulfonylethyl-propion-2-yl)-N-acetyl-α-D-glucosamine

Guidance literature:: Multi-step reaction with 3 steps

1: aq. AcOH / Heating

2: pyridine

3: 53 percent / H₂; AcOH / Pd/C / 775.74 Torr

With pyridine; hydrogen; acetic acid; palladium on activated charcoal;
DOI:10.1021/ja016082o

Reference yield:

: 73089-68-6
benzyl 2-acetamido-4,6-O-benzylidene-3-O-[(R)-1-carboxyethyl]-2-deoxy-α-D-glucopyranoside

: 359773-59-4
4,6-O-diacetyl-3-O-((R)-phenylsulfonylethyl-propion-2-yl)-N-acetyl-α-D-glucosamine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / EDCI; DMAP / CH₂Cl₂

2: aq. AcOH / Heating

3: pyridine

4: 53 percent / H₂; AcOH / Pd/C / 775.74 Torr

With pyridine; dmap; hydrogen; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In dichloromethane;
DOI:10.1021/ja016082o