N,N'-<(benzyloxy)carbonyl>actinamine

Base Information

Chemical Name:N,N'-<(benzyloxy)carbonyl>actinamine
CAS No.:64979-02-8
Molecular Formula:C₂₄H₃₀N₂O₈
Molecular Weight:474.511
Hs Code.:

Synonyms:N,N'-<(benzyloxy)carbonyl>actinamine

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Chemical Property of N,N'-<(benzyloxy)carbonyl>actinamine

Chemical Property:

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Technology Process of N,N'-<(benzyloxy)carbonyl>actinamine

There total 11 articles about N,N'-<(benzyloxy)carbonyl>actinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 78436-36-9
4-O-methanesulfonyl-N,N'-<(benzyloxy)carbonyl>-4-(S)-dihydrospectinomycin

: 64979-02-8
N,N'-<(benzyloxy)carbonyl>actinamine

: 56733-82-5,56782-21-9,58560-42-2,68889-79-2
N,N'-<(benzyloxy)carbonyl>-4(R)-dihydrospectinomycin

Guidance literature:: With silver carbonate; In water; acetone; Heating;
DOI:10.1139/v85-026

Reference yield:

: 96681-00-4
4-O-acetyl-N,N'-<(benzyloxy)carbonyl>-4(R)-dihydrospectinomycin

: 64979-02-8
N,N'-<(benzyloxy)carbonyl>actinamine

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) 1N sodium methoxyde (pH 8); 2.) Dowex-50 (H+) / methanol / 0.25 h / 25 °C

2: 80 percent / 1.) bis(tri-n-butyltin)oxide, 2.)NBS / benzene / 25 °C / 1.) 1 h, 2.) 10 h

3: 90 percent / H₂ / palladium-on-charcoal / H₂O; propan-2-ol

4: Dowex-1 (OH-)

5: H₂ / catalytic hydrogenation

6: 97 percent / pyridine / 18 h / 0 °C

7: 9 percent / silver carbonate / acetone; H₂O

With N-Bromosuccinimide; Dowex-1 (OH-); Dowex-50 (H+); hydrogen; sodium methylate; silver carbonate; bis(tri-n-butyltin)oxide; palladium on activated charcoal; In pyridine; methanol; water; isopropyl alcohol; acetone; benzene;
DOI:10.1139/v85-026

Reference yield:

: 56733-83-6,58560-43-3,68889-80-5
N,N'-<(benzyloxy)carbonyl>spectinomycin

: 64979-02-8
N,N'-<(benzyloxy)carbonyl>actinamine

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / H₂ / palladium-on-charcoal / H₂O; propan-2-ol

2: Dowex-1 (OH-)

3: H₂ / catalytic hydrogenation

4: 97 percent / pyridine / 18 h / 0 °C

5: 9 percent / silver carbonate / acetone; H₂O

With Dowex-1 (OH-); hydrogen; silver carbonate; palladium on activated charcoal; In pyridine; water; isopropyl alcohol; acetone;
DOI:10.1139/v85-026