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C23H28O3Si

Base Information
  • Chemical Name:C23H28O3Si
  • CAS No.:1370655-22-3
  • Molecular Formula:C23H28O3Si
  • Molecular Weight:380.559
  • Hs Code.:
C<sub>23</sub>H<sub>28</sub>O<sub>3</sub>Si

Synonyms:C23H28O3Si

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Chemical Property of C23H28O3Si
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Technology Process of C23H28O3Si

There total 1 articles about C23H28O3Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

Guidance literature:
With hydrogen; In methanol; at 20 ℃; for 11h;
DOI:10.1021/jo202602n
Guidance literature:
methyllithium lithium bromide; With copper(l) iodide; In diethyl ether; at -30 - 0 ℃; Inert atmosphere;
C23H28O3Si; In diethyl ether; at -20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo202602n
Guidance literature:
Multi-step reaction with 2 steps
1.1: copper(l) iodide / diethyl ether / -30 - 0 °C / Inert atmosphere
1.2: 1 h / -20 °C / Inert atmosphere
2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
2.2: 0.75 h / Inert atmosphere
With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo202602n
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