C₄₉H₆₆N₆O₆Si

Base Information

Chemical Name:C₄₉H₆₆N₆O₆Si
CAS No.:1419389-63-1
Molecular Formula:C₄₉H₆₆N₆O₆Si
Molecular Weight:863.185
Hs Code.:

C<sub>49</sub>H<sub>66</sub>N<sub>6</sub>O<sub>6</sub>Si

Synonyms:C₄₉H₆₆N₆O₆Si

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Chemical Property of C₄₉H₆₆N₆O₆Si

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Technology Process of C₄₉H₆₆N₆O₆Si

There total 7 articles about C₄₉H₆₆N₆O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.6%

: 1228552-62-2
(S)-2-(4-iodo-1H-imidazol-2-yl)pyrrolidine-1-carboxylic acid tert-butyl ester

: 1419389-61-9
C₄₃H₆₀BN₃O₆Si

: 1419389-63-1
C₄₉H₆₆N₆O₆Si

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; at 90 ℃; for 2h; Inert atmosphere;

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1419389-63-1
C₄₉H₆₆N₆O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: borane-THF / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C

3: ammonia / methanol / 0 - 20 °C

4: N-iodo-succinimide / dichloromethane / 1.5 h / 0 °C

5: sodium sulfite / ethanol; water / 17 h / Reflux

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 2 h / 90 °C / Inert atmosphere

With N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; borane-THF; ammonia; potassium carbonate; Dess-Martin periodane; sodium sulfite; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water;

Reference yield:

: 1419392-83-8
C₃₈H₄₈F₃N₃O₇SSi

: 1419389-63-1
C₄₉H₆₆N₆O₆Si

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 0.5 h / 100 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 2 h / 90 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; In 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;