Benzene-1,3,5-tricarboxylic acid tris-[((S)-2-hydroxy-1-phenyl-ethyl)-amide]

Base Information

• Chemical Name: Benzene-1,3,5-tricarboxylic acid tris-[((S)-2-hydroxy-1-phenyl-ethyl)-amide]
• CAS No.: 365280-02-0
• Molecular Formula: C₃₃H₃₃N₃O₆
• Molecular Weight: 567.642

Synonyms:Benzene-1,3,5-tricarboxylic acid tris-[((S)-2-hydroxy-1-phenyl-ethyl)-amide]

Chemical Property of Benzene-1,3,5-tricarboxylic acid tris-[((S)-2-hydroxy-1-phenyl-ethyl)-amide]

Chemical Property:

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Technology Process of Benzene-1,3,5-tricarboxylic acid tris-[((S)-2-hydroxy-1-phenyl-ethyl)-amide]

There total 2 articles about Benzene-1,3,5-tricarboxylic acid tris-[((S)-2-hydroxy-1-phenyl-ethyl)-amide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1,3,5-benzene tris(carbonyl chloride) (4422-95-1) + (2S)-2-phenylglycinol (20989-17-7) → Benzene-1,3,5-tricarboxylic acid tris-[((S)-2-hydroxy-1-phenyl-ethyl)-amide] (365280-02-0)

Guidance literature:

With triethylamine; In dichloromethane; for 4h; Heating;

DOI:10.1021/ol050047v

Reference yield:

benzene-1,3,5-tricarboxylic acid (554-95-0) → Benzene-1,3,5-tricarboxylic acid tris-[((S)-2-hydroxy-1-phenyl-ethyl)-amide] (365280-02-0)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂; DMF / 6 h / Heating

2: 88 percent / triethylamine / CH₂Cl₂ / 4 h / Heating

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;

DOI:10.1021/ol050047v

Reference yield: 95.0%

Benzene-1,3,5-tricarboxylic acid tris-[((S)-2-hydroxy-1-phenyl-ethyl)-amide] (365280-02-0) → 1,3,5-tris[2-(4-(S)-phenyl-1,3-oxazoline)]benzene (365280-04-2)

Guidance literature:

With methanesulfonyl chloride; triethylamine; In dichloromethane; at 20 ℃; for 30h;

DOI:10.1016/S0040-4039(01)00915-7

upstream raw materials:

1,3,5-benzene tris(carbonyl chloride)

(2S)-2-phenylglycinol

benzene-1,3,5-tricarboxylic acid

Downstream raw materials:

1,3,5-tris[2-(4-(S)-phenyl-1,3-oxazoline)]benzene

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