2-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)ethyl nitrate

Base Information

Chemical Name:2-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)ethyl nitrate
CAS No.:1431987-05-1
Molecular Formula:C₁₄H₁₉NO₈
Molecular Weight:329.307
Hs Code.:

Synonyms:2-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)ethyl nitrate

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Chemical Property of 2-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)ethyl nitrate

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Technology Process of 2-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)ethyl nitrate

There total 6 articles about 2-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)ethyl nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1431987-58-4
2-(3-(2,3,4,5-tetramethoxy-6-methylphenyl)propoxy)ethyl nitrate

: 1431987-05-1
2-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)ethyl nitrate

Guidance literature:: With ammonium cerium (IV) nitrate; In water; acetonitrile; at 0 ℃; for 3h;

Reference yield: 37.0%

: 1431987-60-8
2-[3-(2,3,4,5-tetramethoxy-6-methylphenyl)propoxy]ethanol

: 1431987-05-1
2-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)ethyl nitrate

: 1431987-58-4
2-(3-(2,3,4,5-tetramethoxy-6-methylphenyl)propoxy)ethyl nitrate

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; tetrabutylammonium nitrate; In dichloromethane; at -78 ℃; for 0.5h;

Reference yield:

: 71573-66-5
1‐allyl‐2,3,4,5‐tetramethoxy‐6‐methylbenzene

: 1431987-05-1
2-(3-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dienyl)propoxy)ethyl nitrate

Guidance literature:: Multi-step reaction with 5 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 16 h / 0 - 20 °C

1.2: 0.5 h / 0 °C

2.1: sodium hydride; 15-crown-5 / mineral oil; N,N-dimethyl-formamide / 0.25 h / 0 °C

2.2: 80 °C

3.1: pyridinium p-toluenesulfonate / methanol; chloroform

4.1: 2,6-di-tert-butyl-4-methylpyridine; tetrabutylammonium nitrate; trifluoromethylsulfonic anhydride / dichloromethane / 0.5 h / -78 °C

5.1: ammonium cerium (IV) nitrate / acetonitrile; water / 3 h / 0 °C

With 2,6-di-tert-butyl-4-methylpyridine; ammonium cerium (IV) nitrate; 15-crown-5; trifluoromethylsulfonic anhydride; pyridinium p-toluenesulfonate; tetrabutylammonium nitrate; sodium hydride; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;