2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal

Base Information

Chemical Name:2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal
CAS No.:1075708-96-1
Molecular Formula:C₇₆H₉₀O₁₇S
Molecular Weight:1328.44
Hs Code.:

2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal

Synonyms:2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal

Suppliers and Price of 2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal

There total 1 articles about 2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 4-methoxyphenyl 2-O-(benzyl-d7)-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-(benzyl-d7)-4,6-O-cyclohexylidene-α-D-mannopyranoside

: 1075708-62-1
methyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-2-O-2-naphthylmethyl-1-thio-β-D-glucopyranoside

: 1075708-96-1
2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 23h; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.200800249

Reference yield: 85.0%

: 1075708-96-1
2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal

: 108-24-7
acetic anhydride

: 1075708-97-2
4-methoxyphenyl 2-O-acetyl-3-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-mannopyranoside

Guidance literature:: 2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal; With 2,6-di-tert-butyl-4-methylpyridine; methyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 20 ℃; for 7h; Molecular sieve; Inert atmosphere;

acetic anhydride; With pyridine; dmap; at 20 ℃; for 14h;
DOI:10.1002/ejoc.200800249

Reference yield: 76.0%

: 1075708-96-1
2-naphthaldehyde (4-methoxyphenyl 2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3')-2'-O-[D7]benzyl-4',6'-O-cyclohexylidene-α-D-mannopyranosid-3-yl) (methyl 3-O-[D7]benzyl-4,6-O-cyclohexyliene-1-thio-β-D-glucopyranosid-2-yl) acetal

: 4-methoxyphenyl 3-O-(benzyl-d7)-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-(benzyl-d7)-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-(benzyl-d7)-4,6-O-cyclohexylidene-α-D-mannopyranoside

: 1075708-99-4
4-methoxyphenyl 3-O-[D7]benzyl-4,6-O-cyclohexylidene-2-O-(2-naphthylmethyl)-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-glucopyranosyl-(1->3)-2-O-[D7]benzyl-4,6-O-cyclohexylidene-α-D-mannopyranoside

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; tris-(trimethylsilyl)silane; methyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 20 ℃; for 14h; Molecular sieve; Inert atmosphere;
DOI:10.1002/ejoc.200800249