Mo₂Cl₆(bis(diphenylphosphino)methane)2

Base Information

Chemical Name:Mo₂Cl₆(bis(diphenylphosphino)methane)2
CAS No.:99808-51-2
Molecular Formula:C₅₀H₄₄Cl₆Mo₂P₄
Molecular Weight:1173.39
Hs Code.:

Mo<sub>2</sub>Cl<sub>6</sub>(bis(diphenylphosphino)methane)2

Synonyms:Mo₂Cl₆(bis(diphenylphosphino)methane)2

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Chemical Property of Mo₂Cl₆(bis(diphenylphosphino)methane)2

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Technology Process of Mo₂Cl₆(bis(diphenylphosphino)methane)2

There total 2 articles about Mo₂Cl₆(bis(diphenylphosphino)methane)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 64508-35-6
Mo₂Cl₄(bis(diphenylphosphino)methane)2

: 99808-51-2
Mo₂Cl₆(bis(diphenylphosphino)methane)2

Guidance literature:: With Cl₂; In dichloromethane; colour of the soln.: green -> bright red; washed with diethyl ether;

Reference yield:

: tetrapotassium octachlorodimolybdate(II)

: 28926-65-0
Tris(diphenylphosphino)methan

: 99808-51-2
Mo₂Cl₆(bis(diphenylphosphino)methane)2

Guidance literature:: In tetrahydrofuran; methanol; Mo2Cl6(dppm)2 was obtained as a minor product in the reaction of K4Mo2Cl8 with HC(PPh2)3 in refluxing MeOH-THF (1:1 v/v) under Ar; unreproducible prepn.; identified by a comparison between the X-ray diffraction powder pattern calcd. from the single crystal data with that obtained by using a sample prepared by the Wilkinson method (Wilkinson et al., Polyhedron, (1984), 3, 347);
DOI:10.1021/ja00265a022