2,4-di(tert-butyl)-7-(4-nitrobenzoyl)-6,7-dihydrofuro-[2',3':3,4]cyclohepta[1,2-b]indole

Base Information

Chemical Name:2,4-di(tert-butyl)-7-(4-nitrobenzoyl)-6,7-dihydrofuro-[2',3':3,4]cyclohepta[1,2-b]indole
CAS No.:1234715-29-7
Molecular Formula:C₃₀H₃₀N₂O₄
Molecular Weight:482.579
Hs Code.:

Synonyms:2,4-di(tert-butyl)-7-(4-nitrobenzoyl)-6,7-dihydrofuro-[2',3':3,4]cyclohepta[1,2-b]indole

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Chemical Property of 2,4-di(tert-butyl)-7-(4-nitrobenzoyl)-6,7-dihydrofuro-[2',3':3,4]cyclohepta[1,2-b]indole

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Technology Process of 2,4-di(tert-butyl)-7-(4-nitrobenzoyl)-6,7-dihydrofuro-[2',3':3,4]cyclohepta[1,2-b]indole

There total 5 articles about 2,4-di(tert-butyl)-7-(4-nitrobenzoyl)-6,7-dihydrofuro-[2',3':3,4]cyclohepta[1,2-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1234715-26-4
bis(5-tert-butyl-2-furyl){2-[(4-nitrobenzoyl)amino]-phenyl}methane

: 1234715-29-7
2,4-di(tert-butyl)-7-(4-nitrobenzoyl)-6,7-dihydrofuro-[2',3':3,4]cyclohepta[1,2-b]indole

: 1234715-28-6
1-[3-(5-tert-butyl-2-furyl)-1-(4-nitrobenzoyl)-1H-indol-2-yl]-4,4-dimethylpentan-3-one

Guidance literature:: With water; trichlorophosphate; In benzene; at 20 ℃; for 24h;
DOI:10.1007/s10593-010-0477-2

Reference yield:

: 7040-43-9
2-tert-butylfuran

: 1234715-29-7
2,4-di(tert-butyl)-7-(4-nitrobenzoyl)-6,7-dihydrofuro-[2',3':3,4]cyclohepta[1,2-b]indole

: 1234715-28-6
1-[3-(5-tert-butyl-2-furyl)-1-(4-nitrobenzoyl)-1H-indol-2-yl]-4,4-dimethylpentan-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: perchloric acid / 1,4-dioxane

2: hydrazine

3: benzene / 1 h / 20 °C

4: trichlorophosphate / water; benzene / 24 h / 20 °C

With perchloric acid; hydrazine; trichlorophosphate; In 1,4-dioxane; water; benzene;
DOI:10.1002/jhet.635

Reference yield:

: 920455-02-3
C₂₃H₂₉NO₂

: 1234715-29-7
2,4-di(tert-butyl)-7-(4-nitrobenzoyl)-6,7-dihydrofuro-[2',3':3,4]cyclohepta[1,2-b]indole

: 1234715-28-6
1-[3-(5-tert-butyl-2-furyl)-1-(4-nitrobenzoyl)-1H-indol-2-yl]-4,4-dimethylpentan-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 1 h / 20 °C

2: trichlorophosphate / water; benzene / 24 h / 20 °C

With trichlorophosphate; In water; benzene;
DOI:10.1002/jhet.635