tris(5-tert-butyl-3,4-dimethoxyphenyl)carbinol

Base Information

Chemical Name:tris(5-tert-butyl-3,4-dimethoxyphenyl)carbinol
CAS No.:353524-69-3
Molecular Formula:C₃₇H₅₂O₇
Molecular Weight:608.816
Hs Code.:

Synonyms:tris(5-tert-butyl-3,4-dimethoxyphenyl)carbinol

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Chemical Property of tris(5-tert-butyl-3,4-dimethoxyphenyl)carbinol

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Technology Process of tris(5-tert-butyl-3,4-dimethoxyphenyl)carbinol

There total 1 articles about tris(5-tert-butyl-3,4-dimethoxyphenyl)carbinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 616-38-6
carbonic acid dimethyl ester

: 168985-94-2
4-bromo-6-tert-butylcatechol dimethyl ether

: 353524-69-3
tris(5-tert-butyl-3,4-dimethoxyphenyl)carbinol

Guidance literature:: 4-bromo-6-tert-butylcatechol dimethyl ether; With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 1.25h;

carbonic acid dimethyl ester; In tetrahydrofuran; at -78 - 20 ℃; for 36h; Further stages.;
DOI:10.1021/ja010630g

Reference yield:

: 353524-69-3
tris(5-tert-butyl-3,4-dimethoxyphenyl)carbinol

: C₃₇H₅₁O₆⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: With tetrafluoroboric acid; acetic anhydride; In water;
DOI:10.1021/ja010630g

Reference yield:

: 353524-69-3
tris(5-tert-butyl-3,4-dimethoxyphenyl)carbinol

: C₃₂H₃₆O₆

Guidance literature:: Multi-step reaction with 4 steps

1: acetic anhydride; HBF₄ / H₂O

2: 470 mg / tetrahydrofuran / -78 - 20 °C

3: BBr₃ / CH₂Cl₂ / -78 - 20 °C

4: 84 percent / Fetizon's reagent / tetrahydrofuran

With tetrafluoroboric acid; acetic anhydride; boron tribromide; silver carbonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja010630g