2,3,4-Tri-O-benzyl-5,6-dideoxy-D-xylo-hex-5-enose oxime

Base Information

Chemical Name:2,3,4-Tri-O-benzyl-5,6-dideoxy-D-xylo-hex-5-enose oxime
CAS No.:219586-93-3
Molecular Formula:C₂₇H₂₉NO₄
Molecular Weight:431.532
Hs Code.:

Synonyms:2,3,4-Tri-O-benzyl-5,6-dideoxy-D-xylo-hex-5-enose oxime

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Chemical Property of 2,3,4-Tri-O-benzyl-5,6-dideoxy-D-xylo-hex-5-enose oxime

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Technology Process of 2,3,4-Tri-O-benzyl-5,6-dideoxy-D-xylo-hex-5-enose oxime

There total 6 articles about 2,3,4-Tri-O-benzyl-5,6-dideoxy-D-xylo-hex-5-enose oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 73111-58-7,130861-06-2,73111-15-6
2,3,4-tri-O-benzyl-5,6-dideoxy-D-xylo-hex-5-enose

: 219586-93-3
2,3,4-Tri-O-benzyl-5,6-dideoxy-D-xylo-hex-5-enose oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium hydrogencarbonate; In methanol; Reflux;
DOI:10.1002/cmdc.201700558

Reference yield:

: 85716-43-4
methyl 6-deoxy-6-iodo-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 219586-93-3
2,3,4-Tri-O-benzyl-5,6-dideoxy-D-xylo-hex-5-enose oxime

Guidance literature:: Multi-step reaction with 2 steps

1: Zn / aq. ethanol / 2 h / Heating

2: NH₂OH*HCl; Na₂CO₃ / methanol / 12 h / 20 °C

With hydroxylamine hydrochloride; sodium carbonate; zinc; In methanol; ethanol; 1: Ring cleavage / 2: Condensation;
DOI:10.1016/S0040-4020(99)00991-6

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 219586-93-3
2,3,4-Tri-O-benzyl-5,6-dideoxy-D-xylo-hex-5-enose oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / Reflux

2: zinc / tetrahydrofuran; water / Sonication

3: sodium hydrogencarbonate; hydroxylamine hydrochloride / methanol / Reflux

With 1H-imidazole; hydroxylamine hydrochloride; iodine; sodium hydrogencarbonate; triphenylphosphine; zinc; In tetrahydrofuran; methanol; water;
DOI:10.1002/cmdc.201700558