sodium 3-(2-amino-6,6-dimethyl-8-oxo-9-phenyl-5,7,8,9-tetrahydro[1,2,4]triazolo[5,1-b]quinazolin-3(6H)-yl)propanoate

Base Information

Chemical Name:sodium 3-(2-amino-6,6-dimethyl-8-oxo-9-phenyl-5,7,8,9-tetrahydro[1,2,4]triazolo[5,1-b]quinazolin-3(6H)-yl)propanoate
CAS No.:1534330-52-3
Molecular Formula:C₂₀H₂₂N₅O₃*Na
Molecular Weight:403.416
Hs Code.:

Synonyms:sodium 3-(2-amino-6,6-dimethyl-8-oxo-9-phenyl-5,7,8,9-tetrahydro[1,2,4]triazolo[5,1-b]quinazolin-3(6H)-yl)propanoate

Suppliers and Price of sodium 3-(2-amino-6,6-dimethyl-8-oxo-9-phenyl-5,7,8,9-tetrahydro[1,2,4]triazolo[5,1-b]quinazolin-3(6H)-yl)propanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of sodium 3-(2-amino-6,6-dimethyl-8-oxo-9-phenyl-5,7,8,9-tetrahydro[1,2,4]triazolo[5,1-b]quinazolin-3(6H)-yl)propanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of sodium 3-(2-amino-6,6-dimethyl-8-oxo-9-phenyl-5,7,8,9-tetrahydro[1,2,4]triazolo[5,1-b]quinazolin-3(6H)-yl)propanoate

There total 3 articles about sodium 3-(2-amino-6,6-dimethyl-8-oxo-9-phenyl-5,7,8,9-tetrahydro[1,2,4]triazolo[5,1-b]quinazolin-3(6H)-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1534330-34-1
8,8-dimethyl-2,10-dioxo-11-phenyl-1,2,3,4,6,7,8,9,10,11-decahydropyrimido[2',1':3,4][1,2,4]triazolo[5,1-b]quinazolin-12-ium chloride

: 1534330-52-3
sodium 3-(2-amino-6,6-dimethyl-8-oxo-9-phenyl-5,7,8,9-tetrahydro[1,2,4]triazolo[5,1-b]quinazolin-3(6H)-yl)propanoate

Guidance literature:: With sodium carbonate; In water; for 2h; Reflux;
DOI:10.1016/j.tet.2013.11.090

Reference yield:

: 872410-93-0
2-amino-6,6-dimethyl-9-phenyl-5,6,7,9-tetrahydro[1,2,4]triazolo[5,1-b]quinazolin-8(4H)-one

: 1534330-52-3
sodium 3-(2-amino-6,6-dimethyl-8-oxo-9-phenyl-5,7,8,9-tetrahydro[1,2,4]triazolo[5,1-b]quinazolin-3(6H)-yl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / N,N-dimethyl-formamide; acetonitrile / 0.25 h / 20 °C

2: N,N-dimethyl-formamide; acetonitrile / 4 h / 80 - 90 °C

3: sodium carbonate / water / 2 h / Reflux

With pyridine; sodium carbonate; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2013.11.090

Reference yield:

: C₂₀H₂₂ClN₅O₂

: 1534330-52-3
sodium 3-(2-amino-6,6-dimethyl-8-oxo-9-phenyl-5,7,8,9-tetrahydro[1,2,4]triazolo[5,1-b]quinazolin-3(6H)-yl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide; acetonitrile / 4 h / 80 - 90 °C

2: sodium carbonate / water / 2 h / Reflux

With sodium carbonate; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2013.11.090