N⁴-benzoyl-1-(2,3-di-O-benzoyl-β-D-arabinofuranosyl)cytosine 5'-[(prop-3-yl hepta-O-acetyl-β-lactoside)-1-yl] phosphonate

Base Information

• Chemical Name: N⁴-benzoyl-1-(2,3-di-O-benzoyl-β-D-arabinofuranosyl)cytosine 5'-[(prop-3-yl hepta-O-acetyl-β-lactoside)-1-yl] phosphonate
• CAS No.: 196083-28-0
• Molecular Formula: C₅₉H₆₆N₃O₂₈P
• Molecular Weight: 1296.15

Synonyms:N⁴-benzoyl-1-(2,3-di-O-benzoyl-β-D-arabinofuranosyl)cytosine 5'-[(prop-3-yl hepta-O-acetyl-β-lactoside)-1-yl] phosphonate

Chemical Property of N⁴-benzoyl-1-(2,3-di-O-benzoyl-β-D-arabinofuranosyl)cytosine 5'-[(prop-3-yl hepta-O-acetyl-β-lactoside)-1-yl] phosphonate

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Technology Process of N⁴-benzoyl-1-(2,3-di-O-benzoyl-β-D-arabinofuranosyl)cytosine 5'-[(prop-3-yl hepta-O-acetyl-β-lactoside)-1-yl] phosphonate

There total 1 articles about N⁴-benzoyl-1-(2,3-di-O-benzoyl-β-D-arabinofuranosyl)cytosine 5'-[(prop-3-yl hepta-O-acetyl-β-lactoside)-1-yl] phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(3-hydroxy-propoxy)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester (196083-23-5) + C30H26N3O10P*C6H15N → N4-benzoyl-1-(2,3-di-O-benzoyl-β-D-arabinofuranosyl)cytosine 5'-[(prop-3-yl hepta-O-acetyl-β-lactoside)-1-yl] phosphonate (196083-28-0)

Guidance literature:

With pyridine; pivaloyl chloride; In acetonitrile; for 0.0833333h; Ambient temperature;

DOI:10.1016/S0008-6215(97)00137-7

Reference yield: 60.0%

N4-benzoyl-1-(2,3-di-O-benzoyl-β-D-arabinofuranosyl)cytosine 5'-[(prop-3-yl hepta-O-acetyl-β-lactoside)-1-yl] phosphonate (196083-28-0) → N4-benzoyl-1-(2,3-di-O-benzoyl-β-D-arabinofuranosyl)cytosine 5'-[(prop-3-yl hepta-O-acetyl-β-lactoside)-1-yl] phosphate (196083-30-4)

Guidance literature:

With iodine; bis-(trimethylsilyl)acetamide; triethylamine; In tetrahydrofuran; for 4h; Ambient temperature;

DOI:10.1016/S0008-6215(97)00137-7

upstream raw materials:

Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(3-hydroxy-propoxy)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

Downstream raw materials:

N⁴-benzoyl-1-(2,3-di-O-benzoyl-β-D-arabinofuranosyl)cytosine 5'-[(prop-3-yl hepta-O-acetyl-β-lactoside)-1-yl] phosphate

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