2-methoxy-5-(4-bromophenyl)benzene sulfonyl chloride

Base Information

Chemical Name:2-methoxy-5-(4-bromophenyl)benzene sulfonyl chloride
CAS No.:189277-77-8
Molecular Formula:C₁₃H₁₀BrClO₃S
Molecular Weight:361.644
Hs Code.:

Synonyms:2-methoxy-5-(4-bromophenyl)benzene sulfonyl chloride

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Chemical Property of 2-methoxy-5-(4-bromophenyl)benzene sulfonyl chloride

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Technology Process of 2-methoxy-5-(4-bromophenyl)benzene sulfonyl chloride

There total 1 articles about 2-methoxy-5-(4-bromophenyl)benzene sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29558-77-8
4-bromo-4'-hydroxybiphenyl

: 189277-77-8
2-methoxy-5-(4-bromophenyl)benzene sulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone

2: ClSO₃H / 3 h / Ambient temperature

With chlorosulfonic acid; potassium carbonate; In acetone;
DOI:10.1016/S0040-4020(97)00134-8

Reference yield:

: 189277-77-8
2-methoxy-5-(4-bromophenyl)benzene sulfonyl chloride

: (1R,2R)-(+)-1,2-[5,5'-di-(4-bromophenyl)-2,2'-dihydroxydibenzenesulfonamido]cyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂

2: NaSPh / dimethylformamide / 4 h / 160 °C

With sodium thiophenolate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00134-8