(⁽¹⁵⁾N₂)monotritylethylenediamine

Base Information

• Chemical Name: (⁽¹⁵⁾N₂)monotritylethylenediamine
• CAS No.: 186972-97-4
• Molecular Formula: C₂₁H₂₂N₂
• Molecular Weight: 304.406
• Mol file: 186972-97-4.mol

Synonyms:(⁽¹⁵⁾N₂)monotritylethylenediamine

Chemical Property of (⁽¹⁵⁾N₂)monotritylethylenediamine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (⁽¹⁵⁾N₂)monotritylethylenediamine

There total 1 articles about (⁽¹⁵⁾N₂)monotritylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.9%

((15)N2)tritylglycinamide (190787-45-2) → ((15)N2)monotritylethylenediamine (186972-97-4)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 48h; Ambient temperature;

DOI:10.1055/s-1997-1208

Reference yield: 96.2%

((15)N2)monotritylethylenediamine (186972-97-4) → 15N-1,2-ethanediamine dihydrochloride (84050-98-6)

Guidance literature:

With hydrogenchloride; for 2h; Heating;

DOI:10.1055/s-1997-1208

Reference yield:

((15)N2)monotritylethylenediamine (186972-97-4) + C24H23(15)NO4 → 1-[((15)N)tritylglycyl]-2-[((15)N2)monotrityl]ethylenediamine

Guidance literature:

In chloroform; Ambient temperature;

DOI:10.1039/a606275j

upstream raw materials:

(⁽¹⁵⁾N₂)tritylglycinamide

Downstream raw materials:

¹⁵N-1,2-ethanediamine dihydrochloride

Refernces

• 1、 Guo, Zijian,Sadler, Peter J.,Zang, Erle. "Recognition of platinum(II) amine complexes by nucleotides: Role of phosphate and carbonyl groups in ([15N3]diethylenetriamine)-(guanosine 5′-monophosphate)platinum(II)". . p. 27 - 28. Retrieved 2007/10/03.