(S)-3-(phenylsulfonyl)-4-(2,2,6-trimethyl-4,7-dioxo-3,8,11-trioxa-5-azatridecan-13-yloxy)-1,2,5-oxadiazol-2-oxide

Base Information

• Chemical Name: (S)-3-(phenylsulfonyl)-4-(2,2,6-trimethyl-4,7-dioxo-3,8,11-trioxa-5-azatridecan-13-yloxy)-1,2,5-oxadiazol-2-oxide
• CAS No.: 1103594-33-7
• Molecular Formula: C₂₀H₂₇N₃O₁₀S
• Molecular Weight: 501.514

Synonyms:(S)-3-(phenylsulfonyl)-4-(2,2,6-trimethyl-4,7-dioxo-3,8,11-trioxa-5-azatridecan-13-yloxy)-1,2,5-oxadiazol-2-oxide

Chemical Property of (S)-3-(phenylsulfonyl)-4-(2,2,6-trimethyl-4,7-dioxo-3,8,11-trioxa-5-azatridecan-13-yloxy)-1,2,5-oxadiazol-2-oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of (S)-3-(phenylsulfonyl)-4-(2,2,6-trimethyl-4,7-dioxo-3,8,11-trioxa-5-azatridecan-13-yloxy)-1,2,5-oxadiazol-2-oxide

There total 1 articles about (S)-3-(phenylsulfonyl)-4-(2,2,6-trimethyl-4,7-dioxo-3,8,11-trioxa-5-azatridecan-13-yloxy)-1,2,5-oxadiazol-2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

4-(2-(2-hydroxyethoxy)ethoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide + L-N-Boc-Ala (15761-38-3) → (S)-3-(phenylsulfonyl)-4-(2,2,6-trimethyl-4,7-dioxo-3,8,11-trioxa-5-azatridecan-13-yloxy)-1,2,5-oxadiazol-2-oxide (1103594-33-7)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;

DOI:10.1016/j.bmc.2010.03.077

Reference yield:

(S)-3-(phenylsulfonyl)-4-(2,2,6-trimethyl-4,7-dioxo-3,8,11-trioxa-5-azatridecan-13-yloxy)-1,2,5-oxadiazol-2-oxide (1103594-33-7) → C15H19N3O8S (1103594-45-1)

Guidance literature:

(S)-3-(phenylsulfonyl)-4-(2,2,6-trimethyl-4,7-dioxo-3,8,11-trioxa-5-azatridecan-13-yloxy)-1,2,5-oxadiazol-2-oxide; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

With triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1016/j.bmc.2010.03.077

upstream raw materials:

L-N-Boc-Ala

Downstream raw materials:

C₁₅H₁₉N₃O₈S

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