1-[(aminooxy)methyl]-3-nitrobenzene hydrochloride (1:1)

Base Information

Chemical Name:1-[(aminooxy)methyl]-3-nitrobenzene hydrochloride (1:1)
CAS No.:29605-76-3
Molecular Formula:C7H8 N2 O3 . Cl H
Molecular Weight:204.613
Hs Code.:
Mol file:29605-76-3.mol

Synonyms:Hydroxylamine,O-(m-nitrobenzyl)-, monohydrochloride (8CI); Hydroxylamine, O-[(3-nitrophenyl)methyl]-,hydrochloride (9CI); Hydroxylamine, O-(m-nitrobenzyl)-, hydrochloride;m-Nitrobenzyloxyamine hydrochloride

Suppliers and Price of 1-[(aminooxy)methyl]-3-nitrobenzene hydrochloride (1:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-[(aminooxy)methyl]-3-nitrobenzene hydrochloride (1:1)

Chemical Property:

Vapor Pressure:3.23E-05mmHg at 25°C
Boiling Point:355°Cat760mmHg
Flash Point:168.5°C
Density:g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-[(aminooxy)methyl]-3-nitrobenzene hydrochloride (1:1)

There total 3 articles about 1-[(aminooxy)methyl]-3-nitrobenzene hydrochloride (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 30777-84-5
N-(3-nitro-benzyloxy)-phthalimide

: 29605-76-3
O-(3-nitrobenzyl)hydroxylamine hydrochloride

Guidance literature:: N-(3-nitro-benzyloxy)-phthalimide; With hydrazine; In ethanol; dichloromethane; water; for 18h; Heating / reflux;

With hydrogenchloride; In diethyl ether; ethanol;

Reference yield:

: N-(3-nitro-benzyloxy)-benzamide

: 29605-76-3
O-(3-nitrobenzyl)hydroxylamine hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; for 0.25h; Heating;
DOI:10.1016/S0968-0896(99)00090-5

Reference yield:

: 619-23-8
3-Nitrobenzyl chloride

: 29605-76-3
O-(3-nitrobenzyl)hydroxylamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; tetra(n-butyl)ammonium hydrogensulfate / water; dichloromethane / 40 °C

2: acetic acid; hydrogenchloride / water

With hydrogenchloride; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; acetic acid; In dichloromethane; water;
DOI:10.24820/ark.5550190.p010.472