acetyl-lactyl-prolyl-<(N-methyl)-D-leucyl>-threonine methyl ester

Base Information

Chemical Name:acetyl-lactyl-prolyl-<(N-methyl)-D-leucyl>-threonine methyl ester
CAS No.:120448-66-0
Molecular Formula:C₂₂H₃₇N₃O₈
Molecular Weight:471.551
Hs Code.:

Synonyms:acetyl-lactyl-prolyl-<(N-methyl)-D-leucyl>-threonine methyl ester

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Chemical Property of acetyl-lactyl-prolyl-<(N-methyl)-D-leucyl>-threonine methyl ester

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Technology Process of acetyl-lactyl-prolyl-<(N-methyl)-D-leucyl>-threonine methyl ester

There total 1 articles about acetyl-lactyl-prolyl-<(N-methyl)-D-leucyl>-threonine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 535-17-1,3853-80-3,18668-00-3,6034-46-4
(S)-2-acetoxypropionic acid

: 120448-66-0
acetyl-lactyl-prolyl-<(N-methyl)-D-leucyl>-threonine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / (1H-1,2,3-benzotriazol-1-yloxy)-tris(dimethylamino)-phosphonium hexafluorophosphate; diisopropylethylamine / CH₂Cl₂ / 2 h / Ambient temperature

2: 73 percent / trifluoroacetic acid / 2 h / Ambient temperature

3: 1.) N,N'-bis-(2-oxo-3-oxazolidinyl)-phosphonic chloride; triethylamine, 2.) triethylamine / 1.) CH₂Cl₂, room temp., 2.) CH₂Cl₂

With bis(2-oxo-3-oxazolidinyl)phosphoric acid chloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/0040-4020(89)80045-6