benzyl-1-O-[(S)-2-(6-benzyloxycarbonyloxy-2-naphthyl)propionyl]-2,3,4-tri-O-benzyl-β-D-glucopyranuronate

Base Information

Chemical Name:benzyl-1-O-[(S)-2-(6-benzyloxycarbonyloxy-2-naphthyl)propionyl]-2,3,4-tri-O-benzyl-β-D-glucopyranuronate
CAS No.:722535-06-0
Molecular Formula:C₅₅H₅₀O₁₁
Molecular Weight:886.995
Hs Code.:

Synonyms:benzyl-1-O-[(S)-2-(6-benzyloxycarbonyloxy-2-naphthyl)propionyl]-2,3,4-tri-O-benzyl-β-D-glucopyranuronate

Suppliers and Price of benzyl-1-O-[(S)-2-(6-benzyloxycarbonyloxy-2-naphthyl)propionyl]-2,3,4-tri-O-benzyl-β-D-glucopyranuronate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl-1-O-[(S)-2-(6-benzyloxycarbonyloxy-2-naphthyl)propionyl]-2,3,4-tri-O-benzyl-β-D-glucopyranuronate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl-1-O-[(S)-2-(6-benzyloxycarbonyloxy-2-naphthyl)propionyl]-2,3,4-tri-O-benzyl-β-D-glucopyranuronate

There total 4 articles about benzyl-1-O-[(S)-2-(6-benzyloxycarbonyloxy-2-naphthyl)propionyl]-2,3,4-tri-O-benzyl-β-D-glucopyranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 159420-94-7
benzyl <1-O-trichloroethanimidoyl>-2,3,4-tri-O-benzyl-D-glucopyranuronate

: 722535-04-8
(S)-2-(6-benzyloxycarbonyloxy-2-naphthyl)propionic acid

: 722535-06-0
benzyl-1-O-[(S)-2-(6-benzyloxycarbonyloxy-2-naphthyl)propionyl]-2,3,4-tri-O-benzyl-β-D-glucopyranuronate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -30 ℃; for 1h;
DOI:10.1081/CAR-120034003

Reference yield:

: 52079-10-4
(+)-6-O-Demethylnaproxen

: 722535-06-0
benzyl-1-O-[(S)-2-(6-benzyloxycarbonyloxy-2-naphthyl)propionyl]-2,3,4-tri-O-benzyl-β-D-glucopyranuronate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / CH₂Cl₂ / 0.5 h / 20 °C

2: CH₂Cl₂ / 1 h

3: 460 mg / SiO₂ / CH₂Cl₂

4: 67 percent / BF₃*OEt₂ / CH₂Cl₂ / 1 h / -30 °C

With pyridine; boron trifluoride diethyl etherate; silica gel; In dichloromethane;
DOI:10.1081/CAR-120034003

Reference yield:

: C₁₉H₂₆O₃Si

: 722535-06-0
benzyl-1-O-[(S)-2-(6-benzyloxycarbonyloxy-2-naphthyl)propionyl]-2,3,4-tri-O-benzyl-β-D-glucopyranuronate

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 1 h

2: 460 mg / SiO₂ / CH₂Cl₂

3: 67 percent / BF₃*OEt₂ / CH₂Cl₂ / 1 h / -30 °C

With boron trifluoride diethyl etherate; silica gel; In dichloromethane;
DOI:10.1081/CAR-120034003