2-hydroxy-4-methoxymethoxy-6-vinyl-benzoic acid 2-(6-allyl-3-methoxymethoxytetrahydro-pyran-2-yl)-1-methyl-ethyl ester

Base Information

Chemical Name:2-hydroxy-4-methoxymethoxy-6-vinyl-benzoic acid 2-(6-allyl-3-methoxymethoxytetrahydro-pyran-2-yl)-1-methyl-ethyl ester
CAS No.:1301247-83-5
Molecular Formula:C₂₄H₃₄O₈
Molecular Weight:450.529
Hs Code.:

Synonyms:2-hydroxy-4-methoxymethoxy-6-vinyl-benzoic acid 2-(6-allyl-3-methoxymethoxytetrahydro-pyran-2-yl)-1-methyl-ethyl ester

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Chemical Property of 2-hydroxy-4-methoxymethoxy-6-vinyl-benzoic acid 2-(6-allyl-3-methoxymethoxytetrahydro-pyran-2-yl)-1-methyl-ethyl ester

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Technology Process of 2-hydroxy-4-methoxymethoxy-6-vinyl-benzoic acid 2-(6-allyl-3-methoxymethoxytetrahydro-pyran-2-yl)-1-methyl-ethyl ester

There total 17 articles about 2-hydroxy-4-methoxymethoxy-6-vinyl-benzoic acid 2-(6-allyl-3-methoxymethoxytetrahydro-pyran-2-yl)-1-methyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1301247-84-6
7-methoxymethoxy-2,2-dimethyl-5-vinyl-4H-benzo[d][1,3]dioxin-4-one

: 1301247-85-7
1-(6-allyl-3-methoxymethoxy-tetrahydro-pyran-2-yl)-propan-2-ol

: 1301247-83-5
2-hydroxy-4-methoxymethoxy-6-vinyl-benzoic acid 2-(6-allyl-3-methoxymethoxytetrahydro-pyran-2-yl)-1-methyl-ethyl ester

Guidance literature:: 1-(6-allyl-3-methoxymethoxy-tetrahydro-pyran-2-yl)-propan-2-ol; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 ℃; Inert atmosphere;

7-methoxymethoxy-2,2-dimethyl-5-vinyl-4H-benzo[d][1,3]dioxin-4-one; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 35h;
DOI:10.1021/jo200332d

Reference yield:

: 1301247-99-3
C₁₀H₂₀O₅

: 1301247-83-5
2-hydroxy-4-methoxymethoxy-6-vinyl-benzoic acid 2-(6-allyl-3-methoxymethoxytetrahydro-pyran-2-yl)-1-methyl-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / dichloromethane / 3 h / -78 °C / Inert atmosphere

3.1: potassium carbonate / methanol / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0 °C / Inert atmosphere

4.2: 35 h / 20 °C

With pyridine; dmap; boron trifluoride diethyl etherate; sodium hydride; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo200332d

Reference yield:

: 1301247-86-8
acetic acid 6-(2-acetoxy-propyl)-5-methoxymethoxy-tetrahydro-pyran-2-yl ester

: 1301247-83-5
2-hydroxy-4-methoxymethoxy-6-vinyl-benzoic acid 2-(6-allyl-3-methoxymethoxytetrahydro-pyran-2-yl)-1-methyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 3 h / -78 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0 °C / Inert atmosphere

3.2: 35 h / 20 °C

With boron trifluoride diethyl etherate; sodium hydride; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo200332d