C₃₅H₅₃N₅O₈

Base Information

Chemical Name:C₃₅H₅₃N₅O₈
CAS No.:1357008-52-6
Molecular Formula:C₃₅H₅₃N₅O₈
Molecular Weight:671.835
Hs Code.:

C<sub>35</sub>H<sub>53</sub>N<sub>5</sub>O<sub>8</sub>

Synonyms:C₃₅H₅₃N₅O₈

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Chemical Property of C₃₅H₅₃N₅O₈

Chemical Property:

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Technology Process of C₃₅H₅₃N₅O₈

There total 13 articles about C₃₅H₅₃N₅O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1357008-00-4
C₃₆H₅₅N₅O₈

: 1357008-52-6
C₃₅H₅₃N₅O₈

Guidance literature:: C₃₆H₅₅N₅O₈; With dihydrogen peroxide; lithium hydroxide; In methanol; at 0 ℃;

With hydrogenchloride; sodium thiosulfate; In methanol; water; pH=1;
DOI:10.1016/j.tet.2011.11.089

Reference yield:

: 13139-15-6,53296-34-7
N-tert-butoxycarbonyl-L-leucine

: 1357008-52-6
C₃₅H₅₃N₅O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: dihydrogen peroxide; lithium hydroxide / methanol / 0 °C

2.2: pH 1

3.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: dihydrogen peroxide; lithium hydroxide / methanol / 0 °C

4.2: pH 1

5.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

6.1: dihydrogen peroxide; lithium hydroxide / methanol / 0 °C

6.2: pH 1

With dihydrogen peroxide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; dichloromethane;
DOI:10.1016/j.tet.2011.11.089

Reference yield:

: 1357008-12-8
C₂₂H₃₄N₂O₆

: 1357008-52-6
C₃₅H₅₃N₅O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen; palladium / ethanol

2.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.33 h / -47 °C / Inert atmosphere

3.2: -47 - 20 °C

4.1: methoxybenzene; trifluoroacetic acid / dichloromethane

5.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

6.1: dihydrogen peroxide; lithium hydroxide / methanol / 0 °C

6.2: pH 1

With diethylamino-sulfur trifluoride; hydrogen; dihydrogen peroxide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; palladium; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.tet.2011.11.089