Technology Process of C32H43N3O7
There total 8 articles about C32H43N3O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium acetate; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
dimethyl sulfoxide;
at 60 ℃;
for 36h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: benzene / Heating / reflux
2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
2.2: 2 h
3.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C
4.1: trimethylaluminum / hexane; dichloromethane / 0.25 h
4.2: 20 °C
4.3: 2 h
5.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 36 h / 60 °C
With
titanium(IV) isopropylate; trimethylaluminum; potassium acetate; caesium carbonate; pyridine hydrogenfluoride;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; pyridine; hexane; dichloromethane; dimethyl sulfoxide; toluene; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
1.2: 2 h
2.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C
3.1: trimethylaluminum / hexane; dichloromethane / 0.25 h
3.2: 20 °C
3.3: 2 h
4.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 36 h / 60 °C
With
titanium(IV) isopropylate; trimethylaluminum; potassium acetate; caesium carbonate; pyridine hydrogenfluoride;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; pyridine; hexane; dichloromethane; dimethyl sulfoxide; toluene;