(phenyl{[2-(1,1,2,2-tetramethyl-1-silapropoxy)ethyl]amino}methylene)methane-1,1-dicarbonitrile

Base Information

Chemical Name:(phenyl{[2-(1,1,2,2-tetramethyl-1-silapropoxy)ethyl]amino}methylene)methane-1,1-dicarbonitrile
CAS No.:587868-61-9
Molecular Formula:C₁₈H₂₅N₃OSi
Molecular Weight:327.501
Hs Code.:

Synonyms:(phenyl{[2-(1,1,2,2-tetramethyl-1-silapropoxy)ethyl]amino}methylene)methane-1,1-dicarbonitrile

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Chemical Property of (phenyl{[2-(1,1,2,2-tetramethyl-1-silapropoxy)ethyl]amino}methylene)methane-1,1-dicarbonitrile

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Technology Process of (phenyl{[2-(1,1,2,2-tetramethyl-1-silapropoxy)ethyl]amino}methylene)methane-1,1-dicarbonitrile

There total 1 articles about (phenyl{[2-(1,1,2,2-tetramethyl-1-silapropoxy)ethyl]amino}methylene)methane-1,1-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 707-07-3
orthobenzoic acid trimethyl ester

: 587868-61-9
(phenyl{[2-(1,1,2,2-tetramethyl-1-silapropoxy)ethyl]amino}methylene)methane-1,1-dicarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / 4 h / Heating / reflux

2.1: methanol / 0.17 h / 20 °C

2.2: 8 h / 20 °C

In methanol; acetic anhydride;

Reference yield: 65.0%

: 587868-61-9
(phenyl{[2-(1,1,2,2-tetramethyl-1-silapropoxy)ethyl]amino}methylene)methane-1,1-dicarbonitrile

: 96-32-2
bromoacetic acid methyl ester

: 587868-64-2
methyl 3-amino-4-cyano-5-phenyl-1-[2-(1,1,2,2-tetramethyl-1-silapropoxy)ethyl]pyrrole-2-carboxylate

Guidance literature:: With caesium carbonate; In acetonitrile; for 3h; Heating / reflux;

Reference yield:

: 587868-61-9
(phenyl{[2-(1,1,2,2-tetramethyl-1-silapropoxy)ethyl]amino}methylene)methane-1,1-dicarbonitrile

: 5-(2-hydroxyethyl)-4-oxo-6-phenyl-3-hydropyrrolo[3,2-d]pyrimidine-7-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / acetonitrile / 3 h / Heating / reflux

2.1: sodium methylate / methanol; dimethyl sulfoxide / 4 h / 100 °C

2.2: 1 h / 20 °C

With sodium methylate; caesium carbonate; In methanol; dimethyl sulfoxide; acetonitrile;